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Preparation Method of Ultrasonic Dispersion Titanium Carbide Silicon Carbide-Carbon Fiber Friction Material

A titanium carbide silicon carbide and friction material technology, which is applied in the field of friction material preparation, can solve problems such as reduced friction performance and potential safety hazards, and achieve the effects of improving wear resistance and high manufacturing cost.

Inactive Publication Date: 2018-01-12
SHANDONG UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In addition, the friction performance of C / C composite materials will be reduced in a humid environment, which will bring serious safety hazards to the use.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] (1) Set the density to 1.8g / cm 3 The graphitized carbon fiber blanket is fed with a mixed gas of propane gas and nitrogen at a temperature of 900°C. The molar ratio of propane gas: nitrogen is 1:4, the flow rate is controlled at 50ml / min, and the carburizing treatment is performed for 24 hours to obtain a carburized carbon fiber blanket. ;

[0020] (2) Immerse the above carburized carbon fiber blanket into a slurry with a particle size of less than 0.3 μm and a content of 5% titanium carbide, place it in an ultrasonic cleaner and fill it with titanium carbide for 50 minutes, take it out and dry it to obtain a carbon fiber blanket filled with titanium carbide, slurry The material is an aqueous solution containing 1.5% ammonium polyacrylate with a pH value of 9;

[0021] (3) Pass the above-mentioned filled titanium carbide carbon fiber blanket into a mixed gas of trichloromethylsilane gas, hydrogen gas and argon gas at a temperature of 900 °C, and the molar ratio of tric...

Embodiment 2

[0025] (1) Set the density to 0.8g / cm 3 The graphitized carbon fiber blanket is fed with a mixture of propane gas and nitrogen at a temperature of 1000°C. The molar ratio of propane gas: nitrogen is 1:5, the flow rate is controlled at 350ml / min, and the carburizing treatment is performed for 18 hours to obtain a carburized carbon fiber blanket. ;

[0026] (2) Immerse the above carburized carbon fiber blanket into a slurry with a particle size of less than 0.3 μm and a content of 12% titanium carbide, place it in an ultrasonic cleaner and fill it with titanium carbide for 40 minutes, take it out and dry it to obtain a carbon fiber blanket filled with titanium carbide, slurry The material is an aqueous solution containing 1% ammonium polyacrylate with a pH value of 10;

[0027] (3) Pass the above-mentioned filled titanium carbide carbon fiber blanket into a mixed gas of trichloromethylsilane gas, hydrogen gas and argon gas at a temperature of 1000 °C, and the molar ratio of tri...

Embodiment 3

[0031] (1) Set the density to 0.1g / cm 3 The graphitized carbon fiber blanket is passed into a mixed gas of propane gas and nitrogen at a temperature of 1100 ° C. The molar ratio of propane gas: nitrogen is 1: 6, the flow rate is controlled at 600ml / min, and the carburizing treatment is performed for 10 hours to obtain a carburized carbon fiber blanket. ;

[0032] (2) Immerse the above carburized carbon fiber blanket into a slurry with a particle size of less than 0.3 μm and a content of 20% titanium carbide, place it in an ultrasonic cleaner and fill it with titanium carbide for 30 minutes, take it out and dry it to obtain a carbon fiber blanket filled with titanium carbide, slurry The material is an aqueous solution containing 0.5% ammonium polyacrylate with a pH value of 11;

[0033] (3) Pass the above-mentioned filled titanium carbide carbon fiber blanket into a mixed gas of trichloromethylsilane gas, hydrogen gas and argon gas at a temperature of 1100 ° C. The molar ratio...

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Abstract

The invention provides a preparation method for an ultrasonic-dispersed titanium carbide silicon carbide-carbon fiber friction material. The preparation method is characterized by comprising the steps that after carburizing treatment is performed on a graphitized carbon fiber blanket with the density of 0.1-1.8 g / cm<3>, ultrasonic-dispersed titanium carbide filling treatment is performed, silicon carbide depositing treatment is performed, burying siliconizing treatment is performed, and then nitriding treatment is performed in a nitrogen atmosphere to prepare the ultrasonic-dispersed titanium carbide silicon carbide-carbon fiber friction material. According to the preparation method, the graphitized carbon fiber blanket is adopted to achieve preparation of the friction material through the steps of carburizing, titanium carbide filling, silicon carbide depositing, burying siliconizing, nitriding and the like, and the prepared friction material has the high strength, the high toughness and the high friction property and is suitable for various climate conditions.

Description

technical field [0001] The invention relates to a preparation method of a friction material composited by carbon fiber and ceramic material, and belongs to the technical field of composite material preparation. Background technique [0002] At present, carbon fiber and carbon (C / C) composite materials are mainly used as friction materials. Since the wear resistance of C / C composite materials is relatively low, people are looking for a method for preparing friction materials with higher wear resistance. In addition, the friction performance of C / C composite materials will be reduced in a humid environment, which will bring serious safety hazards to the use. Contents of the invention [0003] The object of the present invention is to provide a method for preparing a friction material that can overcome the above-mentioned defects, achieve higher strength, higher friction performance and adapt to various climatic conditions. Its technical solution is: [0004] The preparatio...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B35/80C04B35/584C04B35/565C04B35/56C04B35/634C04B35/65C04B35/622
CPCC04B35/5611C04B35/565C04B35/584C04B35/622C04B35/63424C04B35/65C04B2235/428C04B2235/46
Inventor 唐竹兴
Owner SHANDONG UNIV OF TECH
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