Composite hydrogel contact lens material preparation method
A technology of hydrogel contact lenses and raw materials, applied in glasses/goggles, instruments, optics, etc., can solve the problem of poor mechanical properties of light transmittance lenses, inability to help eyes relieve fatigue, low health care and medicinal value, etc. problems, to achieve the effect of high health care and medicinal value, low expansion rate and good mechanical properties
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Embodiment 1
[0016] (1) Mixing of raw materials: first add cross-linked N-vinylpyrrolidone (NVP) particles into the porogen polyethylene glycol 400 and soak for 2-4 minutes, and then mix with the dissolved quantitative initiator dibenzoyl peroxide Mix HEMA with a glass rod for 1-3 minutes, pour it into a small plastic bag after mixing, put the plastic bag in hot water to fully drive out the gas, and seal the plastic bag after 1-2 minutes of hot water bath Standing up for use, wherein, the mass percentages of the crosslinked N-vinylpyrrolidone (NVP) particles, initiator, HEMA solution and porogen are 5.8%, 0.2%, 36% and 58% respectively;
[0017] (2) Heating reaction: Press the plastic bag sealed in step (1) into a glass mold, then put it into a water bath at 74°C for heating reaction, and control the reaction time to 10 hours;
[0018] (3) Removal of impurities: After the reaction in step (2) is complete, take out the polymer generated in the plastic bag, cut into thin slices, soak the thi...
Embodiment 2
[0020] Example 2: The rest are the same as in Example 1, except that in the step (1), the soaking time is controlled to be 3 minutes, the water bath time is controlled to be 1.5 minutes, and the cross-linked N-vinylpyrrolidone (NVP) particles, initiator, HEMA The mass percentages of the solution and the porogen are 6.7%, 0.3%, 41% and 52% respectively; in the step (2), the temperature of the water bath is controlled to be 76°C, and the reaction time is controlled to be 11h; in the step (3) , the soaking time is controlled to be 6 days; in the step (4), the drying temperature is controlled to be 79° C., and the drying time is controlled to be 19 hours.
Embodiment 3
[0021] Example 3: The rest are the same as in Example 1, except that in the step (1), the soaking time is controlled to be 4 minutes, the water bath time is controlled to be 2 minutes, and the cross-linked N-vinylpyrrolidone (NVP) particles, initiator, HEMA solution The mass percentages of porogen and porogen are 6.9%, 0.1%, 45% and 48% respectively; in the step (2), the temperature of the water bath is controlled to be 75°C, and the reaction time is controlled to be 12h; in the step (3), The soaking time is controlled to be 7 days; in the step (4), the drying temperature is controlled to be 80° C., and the drying time is controlled to be 20 hours.
[0022] After the above process steps, the lens material samples are taken out to be tested:
[0023] serial number Transmittance / % apparent strength Swelling rate / % Comfort Example 1 93.6 it is good 2.0 excellent Example 2 94.3 it is good 2.1 excellent Example 3 93.9 it is good ...
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