Preparation method of synthetic grease dispersed zirconium boride silicon carbide-carbon fiber friction material

A zirconium boride silicon carbide, friction material technology, applied in ceramic products, applications, household appliances, etc., can solve the problems of reduced friction performance, hidden safety hazards, etc., and achieve the effect of improving wear resistance and high manufacturing cost

Inactive Publication Date: 2018-05-25
SHANDONG UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In addition, the friction performance of C / C composite materials will be reduced in a humid environment, which will bring serious safety hazards to the use.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] (1) Set the density to 1.8g / cm 3 The graphitized carbon fiber blanket is fed with a mixed gas of propane gas and nitrogen at a temperature of 900°C. The molar ratio of propane gas: nitrogen is 1:4, the flow rate is controlled at 50ml / min, and the carburizing treatment is performed for 24 hours to obtain a carburized carbon fiber blanket. ;

[0020] (2) Immerse the above-mentioned carburized carbon fiber blanket in a synthetic grease slurry with a particle size of less than 0.3 μm and a content of 5% zirconium boride, place it in an ultrasonic cleaner and fill it with zirconium boride for 50 minutes, take it out and dry it to obtain a filled boride Zirconium carbon fiber blanket, the synthetic fat slurry is an ethanol solution containing 5% synthetic fat;

[0021] (3) Pass the above-mentioned filled zirconium boride carbon fiber blanket into a mixed gas of trichloromethylsilane gas, hydrogen gas and argon gas at a temperature of 900 °C, and the molar ratio of trichlorom...

Embodiment 2

[0025] (1) Set the density to 0.8g / cm 3 The graphitized carbon fiber blanket is fed with a mixture of propane gas and nitrogen at a temperature of 1000°C. The molar ratio of propane gas: nitrogen is 1:5, the flow rate is controlled at 350ml / min, and the carburizing treatment is performed for 18 hours to obtain a carburized carbon fiber blanket. ;

[0026] (2) Immerse the above-mentioned carburized carbon fiber blanket in a synthetic grease slurry with a particle size of less than 0.3 μm and a content of 12% zirconium boride, place it in an ultrasonic cleaner and fill it with zirconium boride for 40 minutes, take it out and dry it to obtain a filled boride Zirconium carbon fiber blanket, synthetic fat slurry is an ethanol solution containing 12% synthetic fat;

[0027] (3) Pass the above-mentioned filled zirconium boride carbon fiber blanket into a mixed gas of trichloromethylsilane gas, hydrogen gas and argon gas at a temperature of 1000 °C, and the molar ratio of trichlorome...

Embodiment 3

[0031] (1) Set the density to 0.1g / cm 3 The graphitized carbon fiber blanket is passed into a mixed gas of propane gas and nitrogen at a temperature of 1100 ° C. The molar ratio of propane gas: nitrogen is 1: 6, the flow rate is controlled at 600ml / min, and the carburizing treatment is performed for 10 hours to obtain a carburized carbon fiber blanket. ;

[0032] (2) Immerse the above-mentioned carburized carbon fiber blanket into a synthetic grease slurry with a particle size of less than 0.3 μm and a content of 20% zirconium boride, place it in an ultrasonic cleaner and fill it with zirconium boride for 30 minutes, take it out and dry it to obtain a filled boride Zirconium carbon fiber blanket, synthetic fat slurry is an ethanol solution containing 20% ​​synthetic fat;

[0033] (3) Pass the above-mentioned filled zirconium boride carbon fiber blanket into a mixed gas of trichloromethylsilane gas, hydrogen gas and argon gas at a temperature of 1100 ° C. The molar ratio of tr...

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Abstract

The invention provides a preparing method for a synthetic fat dispersed zirconium boride silicon carbide-carbon fiber friction material. The preparing method is characterized in that a graphited carbon fiber blanket with the density being 0.1-1.8 g / cm<3> is subjected to synthetic fat dispersed zirconium boride filling treatment after being subjected to carburizing treatment, then silicon carbide deposition treatment is carried out, then burying siliconizing treatment is carried out, and then nitridation treatment is carried out in nitrogen atmosphere, so that the synthetic fat dispersed zirconium boride silicon carbide-carbon fiber friction material is prepared. According to the method, the graphited carbon fiber blanket is adopted for being subjected to carburization, zirconium boride filling, silicon carbide deposition, burying siliconizing, nitridation and the like to prepare the friction material, and the prepared friction material is high in strength, toughness and friction performance, and capable of adapting to various weather conditions.

Description

technical field [0001] The invention relates to a preparation method of a friction material composited by carbon fiber and ceramic material, and belongs to the technical field of composite material preparation. Background technique [0002] At present, carbon fiber and carbon (C / C) composite materials are mainly used as friction materials. Since the wear resistance of C / C composite materials is relatively low, people are looking for a method for preparing friction materials with higher wear resistance. In addition, the friction performance of C / C composite materials will be reduced in a humid environment, which will bring serious safety hazards to the use. Contents of the invention [0003] The object of the present invention is to provide a method for preparing a friction material that can overcome the above-mentioned defects, achieve higher strength, higher friction performance and adapt to various climatic conditions. Its technical solution is: [0004] The preparatio...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B38/00C04B35/80C04B35/58C04B35/573C04B35/591C04B35/65C04B35/622C04B35/565C04B35/632
CPCC04B35/565C04B35/573C04B35/58078C04B35/591C04B35/622C04B35/632C04B35/806C04B38/00C04B2111/00362C04B2111/40C04B2235/46C04B2235/48C04B2235/5248C04B2235/5256C04B2235/616C04B2235/6567C04B2235/658
Inventor 唐竹兴
Owner SHANDONG UNIV OF TECH
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