Method for manufacturing fuel-cell membrane electrode assembly
A technology of fuel cells and manufacturing methods, applied in the direction of fuel cells, bonding methods, film/sheet-shaped adhesives, etc., can solve problems such as reduced production efficiency, achieve improved manufacturing efficiency, prevent deformation and wrinkling, and achieve the desired effect significant effect
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Embodiment 1
[0212] (Preparation of material for adhesive layer formation)
[0213] Put methacrylic acid into the experimental apparatus for polymerization equipped with a 1L round-bottom detachable flask, detachable hood, separatory funnel, thermometer, nitrogen gas introduction tube, Liebig condenser, vacuum seal, stirring rod, and stirring blades 100 parts by weight of lauryl ester (manufactured by Kao Corporation, trade name "EXCEPARLL-MA"), 10.2 parts by weight of 2-hydroxyethyl methacrylate (manufactured by Mitsubishi Rayon Corporation, trade name "ACRYESTERHO"), As a polymerization initiator, 0.22 parts by weight of 2,2'-azobisisobutyronitrile (manufactured by Kishida Chemical Co., Ltd.) and 55 parts by weight of toluene were used to prepare a mixture.
[0214] While stirring the mixture, the inside of the round-bottomed separable flask was replaced with nitrogen at normal temperature. Then, the mixture was stirred at a temperature of 60° C.±2° C. for 12 hours while flowing nitroge...
Embodiment 2
[0226] Put methacrylic acid into the experimental apparatus for polymerization equipped with a 1L round-bottom detachable flask, detachable hood, separatory funnel, thermometer, nitrogen gas introduction tube, Liebig condenser, vacuum seal, stirring rod, and stirring blades 100 parts by weight of lauryl ester (manufactured by Kao Corporation, trade name "EXCEPARLL-MA"), 12.6 parts by weight of 2-hydroxyethyl methacrylate (manufactured by Mitsubishi Rayon Corporation, trade name "ACRYESTERHO"), As a polymerization initiator, 0.23 parts by weight of 2,2'-azobisisobutyronitrile (manufactured by Kishida Chemical Co., Ltd.) and 56 parts by weight of toluene were used to prepare a mixture.
[0227] While stirring the mixture, the inside of the round-bottomed separable flask was replaced with nitrogen at normal temperature. Then, the mixture was stirred at a temperature of 60° C.±2° C. for 12 hours while flowing nitrogen gas, to obtain an intermediate composition containing a methacr...
Embodiment 3
[0235] A pressure-sensitive adhesive sheet A was obtained in the same manner as in Example 1.
[0236] (Evaluation)
[0237] In place of the polymer electrolyte membrane (manufactured by Dupon, trade name "Nafion212CS"), carbon paper (manufactured by SGL Carbon, trade name "10AA") was used as a gas diffusion electrode, and the process was carried out in the same manner as in Example 1. Evaluation corresponding to the step of peeling the pressure-sensitive adhesive sheet.
[0238] As a result, it was confirmed that the carbon paper did not peel off due to its own weight before the ultraviolet irradiation, but it was confirmed that the carbon paper peeled off due to its own weight after the ultraviolet irradiation.
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