Preparation method of peanut-shell degradable nano dust suppressant
A technology for peanut shells and dust suppressants, applied in chemical instruments and methods, other chemical processes, etc., can solve the problems of single effect, high dust suppression efficiency, unsatisfactory dust suppression effect, etc., and achieve the effect of saving resources
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example 1
[0019] Firstly, wash the peanut shells with clean water, grind and sieve after they are naturally dried, and prepare 55-mesh peanut shell powder, which is placed in 5% sodium hydroxide solution according to the solid-to-liquid mass ratio of 1:20 Soak for 1 hour, then heat and stir in a constant temperature water bath at 100°C for 2 hours. After the reaction is complete, filter and collect the filter residue, wash with distilled water until the pH of the filter residue reaches 7.0, and let it dry naturally; Liquid ratio 1:15, put it in a sodium hypochlorite solution with a mass concentration of 1.7%, adjust the pH to 4.5 with glacial acetic acid, then place it in a constant temperature water bath to stir and mix for 3 hours and filter it, collect the filter residue and wash it with distilled water To pH 7.0, dry it naturally to prepare peanut shell cellulose; select 10g of the above-prepared peanut shell cellulose and add 100mL of sulfuric acid with a mass concentration of 30% t...
example 2
[0022]Firstly, wash the peanut shells with clean water, grind and sieve after they are naturally dried, and prepare 58-mesh peanut shell powder, which is placed in 5% sodium hydroxide solution according to the solid-to-liquid mass ratio of 1:20 Soak for 1.5h, then heat and stir in a constant temperature water bath at 100°C for 2.5h, after the reaction is complete, filter and collect the filter residue, wash with distilled water until the pH of the filter residue reaches 7.0 and let it dry naturally; after it dries naturally, According to the solid-to-liquid ratio of 1:15, place it in a sodium hypochlorite solution with a mass concentration of 1.7%, adjust the pH to 4.7 with glacial acetic acid, then place it in a constant temperature water bath to stir and mix for 3.5 hours and filter it to collect the filter residue And wash with distilled water until the pH reaches 7.0, and dry it naturally to prepare peanut shell cellulose; select 11g of the above-prepared peanut shell cellu...
example 3
[0025] Firstly, wash the peanut shells with clean water, and after they are naturally dried, grind and sieve to prepare 60-mesh peanut shell powder, which is placed in 5% sodium hydroxide solution according to the solid-to-liquid mass ratio of 1:20 Soak for 2 hours, then heat and stir in a constant temperature water bath at 100°C for 3 hours. After the reaction is completed, filter and collect the filter residue, wash with distilled water until the pH of the filter residue reaches 7.0 and let it dry naturally; Liquid ratio 1:15, put it in a sodium hypochlorite solution with a mass concentration of 1.7%, adjust the pH to 5.0 with glacial acetic acid, then place it in a constant temperature water bath to stir and mix for 4 hours and filter it, collect the filter residue and wash it with distilled water To pH 7.0, dry it naturally to prepare peanut shell cellulose; select 12g of peanut shell cellulose prepared above and add 110mL of sulfuric acid with a mass concentration of 30% t...
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