Graphene electrolyte for lead-acid storage battery and preparation method of graphene electrolyte
A lead-acid battery and graphene technology, applied in the direction of lead-acid batteries, acid electrolytes, aqueous electrolytes, etc., can solve the problems of poor acid-fixing ability, large electrolyte internal resistance, short service life, etc., to increase the reaction capacity, increase Activation energy, effect of enhancing flow activity
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Embodiment 1
[0029] A kind of lead-acid battery graphene electrolyte, is made up of the component of following mass percent: 0.2% graphene aqueous solution, 0.8% sodium sulfate, 0.1% stannous sulfate, 5% silica sol, 0.5% sodium carboxymethyl cellulose, The remainder is a sulfuric acid solution, and the graphene content of the graphene aqueous solution is 0.5×10 -3 g / ml; SiO in the silica sol 2 The mass percentage content is 10%.
[0030] Graphene is modified before being configured into graphene aqueous solution and comprises the following steps:
[0031] 1) Mix graphene particles, sodium dibutylnaphthalene sulfonate solution with a mass concentration of 15% and acid solution according to a solid-liquid ratio of 1g: 45mL: 18mL, stir and mix for 10min at a controlled temperature of 95°C, filter, and water and no Wash with water and ethanol, and dry in vacuum at 180°C for 15 minutes to obtain primary modified graphene particles;
[0032] 2) Mix primary modified graphene particles with che...
Embodiment 2
[0039] A kind of lead-acid storage battery graphene electrolyte, is made up of the component of following mass percent: 1.5% graphene aqueous solution, 1.5% potassium sulfate, 0.8% sodium sulfate, 0.3% stannous sulfate, 20% silica sol, 3% carboxymethyl Sodium cellulose, the balance is a sulfuric acid solution, and the graphene content of the graphene aqueous solution is 7 × 10 -3 g / ml; SiO in the silica sol 2 The mass percentage content is 15%.
[0040] Graphene is modified before being configured into graphene aqueous solution and comprises the following steps:
[0041]1) Mix graphene particles, sodium dibutylnaphthalene sulfonate solution with a mass concentration of 18% and acid solution at a solid-liquid ratio of 1g: 50mL: 20mL, stir and mix for 15min at a controlled temperature of 110°C, filter, and water and no Wash with water and ethanol, and dry in vacuum at 200°C for 20 minutes to obtain primary modified graphene particles;
[0042] 2) Mix the primary modified grap...
Embodiment 3
[0049] A kind of lead-acid storage battery graphene electrolyte, is made up of the component of following mass percent: 5% graphene aqueous solution, 1.5% sodium sulfate, 1.5% potassium sulfate, 0.8% zinc sulfate, 1.2% aluminum sulfate, 0.7% stannous sulfate , 30% silica sol, 6% sodium carboxymethyl cellulose, and the remainder is sulfuric acid solution, and the graphene content of the graphene aqueous solution is 10×10 -3 g / ml; SiO in the silica sol 2 The mass percentage composition is 23%.
[0050] Graphene is modified before being configured into graphene aqueous solution and comprises the following steps:
[0051] 1) Mix graphene particles, sodium dibutylnaphthalene sulfonate solution with a mass concentration of 20% and acid solution at a material-liquid ratio of 1g: 55mL: 23mL, stir and mix for 25min at a controlled temperature of 120°C, filter, and water and no Washing with water and ethanol, and vacuum drying at 220°C for 25 minutes to obtain primary modified graphen...
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