Photocatalytic concrete material to which titanium dioxide/activated zeolite composite material is sprayed and preparation method of photocatalytic concrete material
一种二氧化钛、活化沸石的技术,应用在催化剂活化/制备、化学仪器和方法、物理/化学过程催化剂等方向,能够解决设备投资大、生产成本高、使用周期短等问题
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preparation example Construction
[0036] Another aspect of the present invention, a preparation method of a photocatalytic concrete material sprayed with titanium dioxide / activated zeolite composite material, comprises the following steps:
[0037] Step S1: Activate the natural zeolite molecular sieve to obtain activated zeolite molecular sieve, which specifically includes washing the natural zeolite molecular sieve with distilled water, putting the cleaned natural zeolite molecular sieve into an oven for drying, and the temperature of the oven is 70-90°C , dried and moved into a high-temperature furnace for calcination to obtain activated activated zeolite molecular sieves.
[0038] Step S2: preparing activated zeolite molecular sieve and tetrabutyl titanate, absolute ethanol, acetic acid, nitric acid and other raw materials into a titanium dioxide / activated zeolite composite material, which specifically includes: step S2a: dissolving tetrabutyl titanate in In water and ethanol, stir to form the first mixture...
Embodiment 1
[0044] A preparation method of a photocatalytic concrete material sprayed with titanium dioxide / activated zeolite composite material (mass ratio is 1:0.5), comprising the following steps:
[0045] (1) The natural zeolite molecular sieve is activated to obtain activated zeolite molecular sieve:
[0046] Wash the natural zeolite molecular sieve with distilled water, then put the cleaned natural zeolite molecular sieve into an oven for drying, the oven temperature is 80°C, after drying, move it into a high-temperature furnace for calcination for 2 hours, and finally obtain an activated zeolite molecular sieve.
[0047] (2) Preparation of titanium dioxide / activated zeolite composite material:
[0048] Dissolve 6ml of tetrabutyl titanate in 24ml of absolute ethanol, mix and stir to form a solution. During the magnetic stirring process, the activated zeolite molecular sieve (5A) was slowly poured into the above mixed solution at a mass ratio of 1:0.5, stirred for 10 minutes, and th...
Embodiment 2
[0056] The difference from Example 1 is that the ratio of titanium dioxide to activated zeolite is 1:1. All other steps are the same.
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