A kind of preparation method of self-adhesive conductive hydrogel
A conductive hydrogel and self-adhesive technology, which is applied in the field of preparation of self-adhesive conductive hydrogel, can solve problems such as increased complexity, achieve good biocompatibility, improve hydrophilicity, and increase dispersibility Effect
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Embodiment 1
[0040] A preparation method of self-adhesive conductive hydrogel, comprising the following steps:
[0041] A, preparation of double-bonded silk fibroin:
[0042] A1: Weigh silk fibroin and dissolve it in water to prepare a solution with a concentration of 2%;
[0043] A2: Slowly add methacrylic anhydride 0.8 times the amount of silk fibroin into the biomacromolecule solution, and then stir and react at 50°C for 24 hours;
[0044] A3: Dilute the reaction solution of silk fibroin and methacrylic anhydride 5 times;
[0045] A4: Place the solution diluted in step A4 in a dialysis bag with a molecular weight cut-off of 12-14 kDa, and dialyze with deionized water to obtain a double-bonded silk fibroin solution;
[0046] A5: Pour the dialyzed solution into a centrifuge tube, centrifuge at 2500rpm for 15 minutes, and freeze-dry the obtained centrifuged precipitate to obtain double-bonded silk fibroin powder.
[0047] B. Preparation of polydopamine-functionalized conductive nanomateri...
Embodiment 2
[0055] A preparation method of self-adhesive conductive hydrogel, comprising the following steps:
[0056] A, prepare double-bonded chitosan:
[0057] A1: Take chitosan and dissolve it in phosphate buffer solution to prepare a solution with a mass concentration of 1%;
[0058] A2: Slowly add methacrylic anhydride 0.16 times the mass of chitosan to the biomacromolecule solution dropwise, then stir and react at 25°C for 24 hours;
[0059] A3: subsequently dilute the reaction solution of chitosan biomacromolecule and methacrylic anhydride 5 times;
[0060] A4: Place the solution diluted in step A4 in a dialysis bag with a molecular weight cut-off of 12 to 14 kDa, and dialyze with deionized water to obtain a double-bonded chitosan solution;
[0061] A5: Pour the dialyzed solution into a centrifuge tube, centrifuge at a speed of 2500 rpm for 15 minutes, and freeze-dry the resulting centrifuged precipitate to obtain a double-bonded chitosan powder.
[0062] B. Preparation of poly...
Embodiment 3
[0070] A preparation method of self-adhesive conductive hydrogel, comprising the following steps:
[0071] A. Preparation of double bonded gelatin:
[0072] A1: Weigh gelatin and dissolve it in phosphate buffer solution to obtain a solution with a gelatin mass concentration of 10%;
[0073] A2: Slowly add glycidyl methacrylate 17.5 times the mass of gelatin to the biomacromolecule solution dropwise, then stir and react at 50°C for 3 hours;
[0074] A3: Then dilute the reaction solution of gelatin and methacrylic anhydride 5 times;
[0075] A4: Place the solution diluted in step A4 in a dialysis bag with a molecular weight cut-off of 12-14 kDa, and dialyze with deionized water to obtain a double-bonded gelatin solution;
[0076] A5: Pour the dialyzed solution into a centrifuge tube, centrifuge at 2500 rpm for 15 minutes, and freeze-dry the resulting centrifuged precipitate to obtain double-bonded gelatin powder.
[0077] B. Preparation of polydopamine-functionalized conducti...
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