Flame retardant thermal insulation polystyrene material and preparation method thereof

A technology of polystyrene, flame retardant and heat preservation, applied in the field of heat preservation materials, can solve the problems of unfavorable EPS board application, etc., and achieve the effects of increasing stability and oxidation resistance, increasing mechanical properties, and increasing smoke suppression

Inactive Publication Date: 2016-08-31
望江县精美欣钢构有限公司
View PDF6 Cites 5 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The "B1 grade EPS board" that appears on the market is made by melting the flame retardant and polystyrene particles and then making the particles into foa

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Flame retardant thermal insulation polystyrene material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0022] Reference figure 1 , The method for preparing a flame-retardant and heat-insulating polystyrene material proposed by the present invention includes the following steps:

[0023] S1. Preparation of polystyrene particles: mix water, polyvinyl alcohol solution, and tricalcium phosphate to obtain solution A; disperse styrene and silica aerogel uniformly by ultrasonic, add triphenyl phosphate and ammonium polyphosphate and mix well , Add di-tert-butyl peroxide and mix well to obtain solution B; mix solution A and solution B evenly, heat up, keep warm and stir, cool down, wash, and air-dry to obtain polystyrene particles;

[0024] S2, pre-expansion and maturation: take the polystyrene particles obtained in S1, adjust the vapor pressure to 0.3-0.5MPa, keep it for 45-55s, take it out, and place it at room temperature for 20-24h to obtain matured particles;

[0025] S3. Foam molding: add water-soluble silicone oil to S2 to obtain mature particles, stir at 500-700r / min for 10-20min, ad...

Example Embodiment

[0027] Example 1

[0028] A flame-retardant and heat-insulating polystyrene material, whose raw materials by weight include: 120 parts of styrene, 200 parts of water, 120 parts of 4wt% polyvinyl alcohol aqueous solution, 3 parts of tricalcium phosphate, and 1.5 parts of triphenyl phosphate. , 2.5 parts of ammonium polyphosphate, 5 parts of silica aerogel, 1 part of di-tert-butyl peroxide, 4 parts of water-soluble silicone oil, 10 parts of pentane, 100 parts of compound flame retardant, 3 parts of benzenesulfonyl chloride , 6 parts of isopropyl triisostearate titanate, 20 parts of fumed white carbon black, 3 parts of rare earth stabilizer, 2 parts of Ca / Zn composite stabilizer, 2645 parts of antioxidant;

[0029] Among them, the preparation method of the compound flame retardant is: adding 15 parts of high polyammonium phosphate, 10 parts of sodium silicate, and 5 parts of montmorillonite to 70 parts of thermosetting phenolic resin by weight parts, stirring at a speed of 400r / min fo...

Example Embodiment

[0034] Example 2

[0035] A flame-retardant and heat-insulating polystyrene material, the raw materials of which include 80 parts by weight of styrene, 400 parts of water, 80 parts of 6wt% polyvinyl alcohol aqueous solution, 5 parts of tricalcium phosphate, and 1 part of triphenyl phosphate. , 4.5 parts of ammonium polyphosphate, 2 parts of silica aerogel, 3 parts of di-tert-butyl peroxide, 2 parts of water-soluble silicone oil, 18 parts of pentane, 80 parts of compound flame retardant, 6 parts of benzenesulfonyl chloride , 4 parts of isopropyl triisostearate titanate, 30 parts of fumed white carbon black, 2 parts of rare earth stabilizer, 3 parts of Ca / Zn composite stabilizer, 2643 parts of antioxidant;

[0036] Among them, the preparation method of the compound flame retardant is: adding 10 parts of high polyammonium phosphate, 7 parts of sodium silicate, and 3 parts of montmorillonite to 60 parts of thermosetting phenolic resin by weight parts, stirring at a speed of 600r / min fo...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention discloses a flame retardant thermal insulation polystyrene material. The raw materials include, by weight, 80-120 parts of styrene, 200-400 parts of water, 80-120 parts of a polyvinyl alcohol solution, 3-5 parts of tricalcium phosphate, 1-1.5 parts of triphenyl phosphate, 2.5-4.5 parts of ammonium polyphosphate, 2-5 parts of silica aerogel, 1-3 parts of di-tert-butyl peroxide, 2-4 parts of water soluble silicone oil, 10-18 parts of pentane, 80-100 parts of a compound flame retardant, 3-6 parts of benzenesulfonyl chloride, 4-6 parts of isopropyl titanate triisostearate, 20-30 parts of fumed silica, 2-3 parts of a rare earth stabilizer, 2-3 parts of a Ca/Zn composite stabilizer, and 3-5 parts of an antioxidant 264. The invention also discloses a preparation method of the flame retardant thermal insulation polystyrene material. The flame retardant thermal insulation polystyrene material provided by the invention has the advantages of simple operation, convenient industrial production, high flame retardance and good thermal insulation performance.

Description

technical field [0001] The invention relates to the technical field of thermal insulation materials, in particular to a flame-retardant thermal insulation polystyrene material and a preparation method thereof. Background technique [0002] Silica airgel is one of the lightest solid nanoporous materials known in the world, with a continuous three-dimensional network structure, it has many special properties, such as ultra-low thermal conductivity, high specific surface area, low density, etc. . It can be used as an interlayer and filling layer for thermal insulation, air purification, water treatment and other functional structures, or it can be used for compounding and bonding with other materials. [0003] Polystyrene (EPS) foam insulation has the advantages of low water absorption, small bulk density, good thermal insulation performance, good mechanical strength and toughness, excellent dielectric properties, corrosion resistance, easy molding and high productivity, and h...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): C08L25/06C08L29/04C08L61/06C08K13/02C08K3/32C08K3/34C08K3/36C08K5/523C08J9/14
CPCC08L25/06C08J9/141C08J2203/14C08J2325/06C08J2329/04C08J2425/06C08J2429/04C08K2201/014C08L29/04C08L2201/02C08L2201/08C08L2201/14C08L2203/14C08L2205/035C08L61/06C08K13/02C08K2003/323C08K3/34C08K3/346C08K3/36C08K5/523
Inventor 聂金红
Owner 望江县精美欣钢构有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap