Bulletproof material introduced with thermosetting epoxy resin and preparation method thereof
An epoxy resin and thermosetting technology, which is applied in the field of bulletproof fiber composite materials, bulletproof materials and their preparation, can solve the problems of insufficient fiber adhesion, unfavorable wearing, insufficient rigidity, etc., and achieves low hygroscopicity, high reactivity, The effect of high curing temperature
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Embodiment 1
[0041] The bulletproof material with thermosetting epoxy resin is introduced, which is a composite material made of matrix resin and fiber;
[0042] The base resin is made of the following raw materials in parts by weight: 10 parts of polyvinyl butyral, 2 parts of epoxy resin, 50 parts of diluent, 1 part of curing agent, and 0.6 parts of auxiliary agent; the base resin, Composite with fibers at a weight ratio of 80:100.
[0043] The molecular weight of described polyvinyl butyral is 100,000;
[0044] Described epoxy resin is bisphenol A type epoxy resin E-51;
[0045] Described diluent is made up of the methanol of 60wt% and the ethanol of 40wt%;
[0046] Described curing agent is dicyandiamide slurry, specifically the mixture that is made up of the epoxy resin of 70wt%, the dicyandiamide of 25wt% and the accelerator of 5wt%;
[0047] The dicyandiamide is an ultrafine powder with a particle size of <10 μm;
[0048] Described accelerator is phenyl dimethyl urea;
[0049] D...
Embodiment 2
[0052] The bulletproof material with thermosetting epoxy resin is introduced, which is a composite material made of matrix resin and fiber;
[0053] The base resin is made of the following raw materials in parts by weight: 13 parts of polyvinyl butyral, 10 parts of epoxy resin, 85 parts of diluent, 8 parts of curing agent, and 0.6 parts of auxiliary agent; the base resin, Composite with fibers at a weight ratio of 70:100.
[0054] The molecular weight of described polyvinyl butyral is 100,000;
[0055] Described epoxy resin is made up of novolac type epoxy resin F-44 and F-51 by equal weight ratio;
[0056] Described diluent is made up of n-butanol, Virahol, toluene in equal weight ratio;
[0057] The curing agent is a phenolic resin with a molecular weight of 500-1000;
[0058] Described auxiliary agent is selected from Corning auxiliary agent Perenol S43;
[0059] The fibers are ultra-high molecular weight polyethylene fibers.
Embodiment 3
[0061] The bulletproof material with thermosetting epoxy resin is introduced, which is a composite material made of matrix resin and fiber;
[0062] The base resin is made of the following raw materials in parts by weight: 18 parts of polyvinyl butyral, 5 parts of epoxy resin, 75 parts of diluent, 6 parts of curing agent, and 0.6 parts of auxiliary agent; the base resin, Composite with fibers at a weight ratio of 60:100.
[0063] The molecular weight of described polyvinyl butyral is 100,000;
[0064] Described epoxy resin is made up of bisphenol A type epoxy resin E-20 and novolak type epoxy resin F-51 by the weight ratio of 1:2;
[0065] Described diluent is made up of acetone, butanone, cyclohexanone, ethyl acetate, propylene glycol methyl ether acetate in equal weight ratio;
[0066] The curing agent is a phenolic resin with a molecular weight of 500-1000;
[0067] Described auxiliary agent is selected from Corning auxiliary agent Texaphor P63;
[0068] The said fiber ...
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