Preparation method of tobacco aroma compensating particles and application thereof to reconstituted tobacco leaves
A technology for flavor compensation and reconstituting tobacco leaves, which is applied in the directions of tobacco, application, and tobacco preparation, can solve problems such as complicated processes, and achieves the effects of simple process method, compensating for the weak flavor of cigarettes, and making up for the loss of tobacco flavor.
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Embodiment 1
[0019] Take 1000g flue-cured tobacco leaf raw material, add water according to the mass ratio of 1:8 to carry out reflux extraction for 2 hours, collect the fraction at 90-110°C by distillation, add dichloromethane to extract the fraction according to the volume ratio of 1:1, and concentrate to remove the dichloromethane to obtain Tobacco flavor absolute; according to the ratio of tobacco stem particles: the mass ratio of tobacco flavor absolute 5:1, adopt 60-80 order tobacco stem particles to absorb tobacco flavor absolute oil for 0.5h and then dry to obtain loaded tobacco flavor absolute Adsorb the particles; then use the saturated aqueous solution method to embed the tobacco stem particles loaded with tobacco flavor absolute with starch, the mass ratio of starch to the tobacco stem particles loaded with tobacco flavor absolute is 2:1, and the embedding time is 2h. The embedding temperature is 60° C., and the tobacco flavor compensating particles are obtained. The prepared t...
Embodiment 2
[0021] Take 1000g of raw flue-cured tobacco leaves, add ethanol according to the mass ratio of 1:8 for reflux extraction for 2 hours, collect fractions at a temperature range of 90-110°C, add 1,2-dichloroethane according to the volume ratio of 1:1 to extract and concentrate the fractions Remove 1,2-dichloroethane to obtain tobacco flavor absolute; according to the mass ratio of hemp stalk core particles: tobacco flavor absolute 10:1, adopt 80-100 mesh hemp stalk core particles to carry out tobacco flavor absolute Dry after adsorption for 1 h; use saturated aqueous solution method to embed the hemp stalk core particles loaded with tobacco flavor absolute with chitosan, and the mass ratio of chitosan to the hemp stalk core particles loaded with tobacco flavor absolute is 5:1 , the embedding time was 2 h, and the embedding temperature was 60° C. to obtain tobacco flavor compensating particles. The tobacco aroma compensating particles are added to the coating liquid according to 2...
Embodiment 3
[0023] Take 1000g of flue-cured tobacco leaf raw material, add ethanol according to the mass ratio of 1:8 for reflux extraction for 2 hours, collect the fraction at 90-110°C by distillation, add ether to extract the fraction according to the volume ratio of 1:1, concentrate and remove the ether, and obtain tobacco aroma absolute ; According to the ratio of bagasse particles: the mass ratio of tobacco flavor absolute oil 15:1, adopt 80-120 order bagasse particles to dry after absorbing tobacco flavor absolute oil for 1.5h; Adopt saturated aqueous solution method, use guar gum and hydroxymethyl The bagasse particles loaded with tobacco flavor absolute were embedded with cellulose sodium, the mass ratio of the total amount of guar gum and sodium hydroxymethyl cellulose to the bagasse particles loaded with tobacco flavor absolute was 7:1, and the embedding time was 2h , the embedding temperature is 60°C, and the tobacco flavor compensating particles are obtained. The tobacco aroma...
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