Polyester-cotton microcapsule disperse reactive dye one-bath dyeing technology

A technology for dispersing active and disperse dyes, applied in the field of dyeing, can solve the problems of no use value, uneven coloring, low color fixing rate, etc., achieve excellent slow release function, good color fastness, avoid influence and hydrolysis damage Effect

Active Publication Date: 2016-12-21
ANHUI YAYUAN PRINTING & DYEING CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] At present, although the disperse dye capsule / reactive dye one-bath dyeing of polyester-cotton fabrics can have the advantage of saving procedures to a certain extent, there are still a lot of problems, such as the limitations of the reactive dyes and disperse dyes used are very large, regardless of Both reactive dyes and disperse dyes require certain specific dyeing performance requirements, which do not have a wide range of use values; and usually there will be problems such as hydrolysis of reactive dyes, uneven coloring, color flowering, color difference, and low color fixation rate.

Method used

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  • Polyester-cotton microcapsule disperse reactive dye one-bath dyeing technology

Examples

Experimental program
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Effect test

Embodiment 1

[0022] In the present embodiment, a kind of polyester-cotton microcapsule disperse reactive dye one-bath dyeing process comprises the following steps:

[0023] S1, dyeing and washing, padding the polyester-cotton fabric to be dyed in the dye solution containing microcapsule disperse dye, the dye solution comprising microcapsule disperse dye includes: microcapsule disperse dye 1% (owf), pH buffer 3g / L. Leveling agent 1g / L, adjust the bath ratio to 1:30, enter dyeing at 20°C, heat up to 65°C at a speed of 3°C / min, keep warm for 10min, and then heat up to 130°C at a speed of 1°C / min, Insulate for 25 minutes, and then cool down to 30°C at a rate of 2°C / min. The microcapsule disperse dye is obtained by using chitosan as the carrier of the disperse dye, and then cross-linked and solidified. The specific preparation method includes: mixing the disperse dye and the shell Add the polysaccharide to the acetic acid solution with a concentration of 0.5wt%, stir evenly, add liquid paraffi...

Embodiment 2

[0027] In the present embodiment, a kind of polyester-cotton microcapsule disperse reactive dye one-bath dyeing process comprises the following steps:

[0028]S1, dyeing and washing, padding the polyester-cotton fabric to be dyed in the dye solution containing microcapsule disperse dye, the dye solution comprising microcapsule disperse dye includes: microcapsule disperse dye 5% (owf), pH buffer 1g / L. Leveling agent 2g / L, adjust the bath ratio to 1:10, enter dyeing at 30°C, heat up to 75°C at a speed of 2°C / min, keep warm for 5min, and then heat up to 110°C at a speed of 2°C / min, Insulate for 45 minutes, then cool down to 40°C at a rate of 1.5°C / min. The microcapsule disperse dye is obtained by using chitosan as the carrier of the disperse dye, and then cross-linked and solidified. The specific preparation method includes: mixing the disperse dye and the shell The polysaccharide was added to the acetic acid solution with a concentration of 3wt% and stirred evenly, then liquid ...

Embodiment 3

[0032] In the present embodiment, a kind of polyester-cotton microcapsule disperse reactive dye one-bath dyeing process comprises the following steps:

[0033] S1, dyeing and washing, padding the polyester-cotton fabric to be dyed in the dye solution containing microcapsule disperse dye, the dye solution comprising microcapsule disperse dye includes: microcapsule disperse dye 2% (owf), pH buffer 2g / L. Leveling agent 1.5g / L, adjust the bath ratio to 1:20, enter dyeing at 25°C, heat up to 70°C at a speed of 2.5°C / min, keep warm for 7 minutes, and then heat up to 120°C at a speed of 1.5°C / min , keep warm for 35min, then cool down to 35°C at a speed of 1.7°C / min, the microcapsule disperse dye adopts chitosan as the carrier of the disperse dye, and then obtains it through cross-linking and solidification. The specific preparation method includes: combining the disperse dye and Chitosan was added to 1.5wt% acetic acid solution and stirred evenly, then liquid paraffin and Tween-80 w...

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Abstract

The invention discloses a polyester-cotton microcapsule disperse reactive dye one-bath dyeing technology. The technology comprises the steps of: S1, polyester dyeing: dipping a to-be-dyed polyester-cotton fabric in a dye solution containing microcapsule disperse dye, conducting heat preservation at 65-75DEG C, then performing heat preservation at 110-130DEG C, and carrying out cooling to 30-40DEG C, using chitosan to serve as the carrier of the disperse dye, and then conducting crosslinking curing; S2. cotton dyeing: adding a quaternary ammonium salt cationic etherifying agent, carrying out stirring reaction, then adding a reactive dye, performing heat preservation at 55-65DEG C, adding an organic solvent, conducting heat preservation at 70-90DEG C, then adding organic amine and sodium carbonate, and performing heat preservation at 60-100DEG C; and S3, aftertreatment: performing cooling to room temperature, and then carrying out primary washing, soaping and after-washing. The polyester-cotton microcapsule disperse reactive dye one-bath dyeing technology provided by the invention has the advantages of simple process, little pollution, wide dye applicability, uniform coloring, high color fixation rate and good level-dyeing properties.

Description

technical field [0001] The invention relates to the technical field of dyeing, in particular to a polyester-cotton microcapsule disperse reactive dye one-bath dyeing process. Background technique [0002] Polyester-cotton blended fabric not only has the function of moisture absorption and breathability of cellulose fiber, but also has good shape retention and color fastness of polyester fiber, so it is favored by consumers and occupies an important position in various clothing fabrics. [0003] The main processes for disperse / reactive dyeing of conventional polyester-cotton blended fabrics are disperse / reactive two-bath method, disperse / reactive one-bath two-step dyeing process and disperse / reactive one-bath one-step dyeing process. These processes have long dyeing time and low production efficiency. , water, electricity, steam consumption is large, and the amount of sewage discharge is large, all of which require reduction cleaning, and reduction cleaning will damage reacti...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06P1/16D06P1/38D06P3/872D06P5/22B01J13/14
CPCB01J13/14D06P1/0016D06P1/16D06P1/38D06P3/8252D06P5/22
Inventor 潘学东
Owner ANHUI YAYUAN PRINTING & DYEING CO LTD
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