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Fine-grained cubic boron nitride blade and preparation method thereof

A boron nitride knife and fine-grained technology, applied in the field of fine-grained cubic boron nitride blades and their preparation, can solve the problems of high price and high production cost

Inactive Publication Date: 2017-01-11
ZHONGNAN DIAMOND CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the purchase and use of foreign fine-grained cubic boron nitride cutting tools is very expensive, resulting in high production costs, while domestic cubic boron nitride cutting tools are limited by the formula and process, and research on fine-grained cubic boron nitride cutting tools and its applications is relatively Western. There is a big gap between developed countries, which is mainly reflected in the tool toughness, tool impact resistance, wear resistance, tool life and machining accuracy.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0022] The preparation method of the above-mentioned fine-grained cubic boron nitride blade comprises the following steps:

[0023] (1) Purification and reduction treatment: Boil cubic boron nitride micropowder with mixed acid solution for 6-7 hours, wash with deionized water until neutral, then boil with aqua regia for 6-7 hours, and wash with deionized water until neutral, then Boil with alkaline solution for 5h~6h, then boil and rinse with deionized water for 9h~10h. The drying time is 10-20 hours; the nano-bonding agent is taken according to the above-mentioned ratio, and it is placed in a hydrogen reduction furnace for reduction treatment. The treatment temperature is 650-750 ° C, and the treatment time is 3-5 hours. After treatment, it is taken out for use; among them :

[0024] The mixed acid solution is prepared by sulfuric acid and nitric acid in a volume ratio of 1:1.2 to 1.5, and the cubic boron nitride micropowder and the mixed acid solution are mixed in a volume ...

Embodiment 1

[0035] A fine-grained cubic boron nitride blade is composed of the following raw materials in weight percentage: 60% of cubic boron nitride micropowder with a particle size of 0.5µm and 40% of nano-bonding agent. The nano-bonding agent is composed of the following raw materials in weight percent: TiN powder 25%, NbC powder 20%, Al 2 o 3 15% powder, 15% HfC powder, 10% Be powder, 10% WC powder and 5% Mo powder, of which, TiN, NbC, Al 2 o 3 and HfC particle size is 10, Be powder, WC powder and Mo powder particle size is 20nm.

[0036] The preparation method of the above-mentioned fine-grained cubic boron nitride blade comprises the following steps:

[0037] (1) Purification and reduction treatment: boil cubic boron nitride micropowder with mixed acid solution for 6 hours, wash with deionized water until neutral, then boil with aqua regia for 6 hours, wash with deionized water until neutral, and then boil with alkali solution 5h, then boil and rinse with deionized water for 9...

Embodiment 2

[0045] A fine-grained cubic boron nitride blade is composed of the following raw materials in weight percentage: 80% of cubic boron nitride micropowder with a particle size of 1 μm and 20% of nano-bonding agent; the nano-bonding agent is composed of the following weight percentage content Raw material composition: TiN powder 45%, NbC powder 17%, Al 2 o 3 12% powder, 12% HfC powder, 6% Be powder, 6% WC powder and 2% Mo powder, among them, TiN, NbC, Al 2 o 3 The particle size of Be and HfC is 20nm, and the particle size of Be powder, WC powder and Mo powder is 30nm.

[0046] The preparation method of the above-mentioned fine-grained cubic boron nitride blade comprises the following steps:

[0047] (1) Purification and reduction treatment: boil cubic boron nitride micropowder with mixed acid solution for 7 hours, wash with deionized water until neutral, then boil with aqua regia for 7 hours, wash with deionized water until neutral, and then wash with alkaline solution Boil fo...

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PUM

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Abstract

The invention relates to a fine-grained cubic boron nitride blade. The blade is prepared from, by weight, 60%-80% of micro cubic boron nitride powder and 20%-40% of nano-binder, wherein the nano-binder is prepared from, by weight, 25%-45% of TiN powder, 17%-20% of NbC powder, 12%-15% of Al2O3 powder, 12%-15% of HfC powder, 6%-10% of Be powder, 6%-10% of WC powder and 2%-5% of Mo power. By adding the nano-binder, formation of a tough sintering body is promoted, the toughness of the cubic boron nitride blade is increased, and the service life is prolonged. According to the fine-grained cubic boron nitride blade prepared through the preparation method, the technical indexes can reach the conditions that the grain size is smaller than or equal to 1 micrometer, the abrasive ratio ranges from 7,000 to 7,500, the microhardness HV ranges from 6,000 to 6,500, and the bending strength ranges from 850 MPa to 900 MPa, and the requirements of precise machining can be met.

Description

technical field [0001] The invention belongs to the technical field of superhard materials, and in particular relates to a fine-grained cubic boron nitride blade and a preparation method thereof. Background technique [0002] With the development of manufacturing technology, cutting processing is developing in the direction of high speed, high precision, and large depth of cut. As one of the most important superhard material cutting tools, cubic boron nitride cutting tools in cutting processing have high hardness, Wear resistance and chemical stability, suitable for machining requirements such as high-speed cutting, hard cutting, dry cutting, etc. Incomparable superiority. [0003] In order to improve the wear resistance, impact toughness and machinability of cubic boron nitride tools, well-known foreign companies have introduced fine-grained tool products with CBN particle sizes below 1 micron or even 0.5 microns. The CBN particle size used by Sumitomo’s BN300 in Japan is ...

Claims

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Application Information

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IPC IPC(8): C04B35/5831C04B35/626C04B35/64
CPCC04B35/5831C04B35/622C04B35/62605C04B35/6261C04B35/64C04B2235/3217C04B2235/3839C04B2235/3847C04B2235/3886C04B2235/40C04B2235/404C04B2235/5436C04B2235/5445C04B2235/656C04B2235/6581C04B2235/661C04B2235/785C04B2235/96C04B2235/963
Inventor 卢灿华张涛窦明刘俊涛
Owner ZHONGNAN DIAMOND CO LTD
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