Preparation method for battery diaphragm with three kinds of microporous structures
A battery diaphragm and microporous structure technology, applied in the field of battery diaphragm preparation, can solve the problems of incomplete sealing of pore forming agents, easy flow out, and difficulty in controlling consistency
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Embodiment 1
[0143] The composition used to prepare three kinds of microporous structure battery diaphragms comprises the following components by weight:
[0144]
[0145] in,
[0146] The number average molecular weight of high molecular polyethylene is 500,000,
[0147] The number average molecular weight of UHMWPE is 1.4 million,
[0148] The average molecular weight of white oil is 200,
[0149] The particle size of the nano-magnesium chloride is 50-70nm.
[0150] Three kinds of microporous structure battery separators were prepared according to the following methods:
[0151] Step 1), extrusion: mix high molecular weight polyethylene and magnesium chloride nanoparticles uniformly, and mix ultra high molecular weight polyethylene, 4,4-thiobis(6-tert-butyl m-cresol), 2,4-dihydroxy Benzophenone, sodium stearyl quaternary ammonium and Tween 80 are mixed evenly, and the above two mixtures are respectively put into the extruder to be heated and melted through two polyethylene composi...
Embodiment 2
[0158] The composition used to prepare three kinds of microporous structure battery diaphragms comprises the following components by weight:
[0159]
[0160] in,
[0161] The number average molecular weight of high molecular weight polyethylene is 300,000,
[0162] The number average molecular weight of UHMWPE is 1.3 million,
[0163] The average molecular weight of white oil is 180,
[0164] The particle size of the nano-magnesium chloride is 60-90nm.
[0165] Three kinds of microporous structure battery separators were prepared according to the following methods:
[0166] Step 1), extrusion: mix high molecular polyethylene and magnesium chloride nanoparticles evenly, and ultra high molecular polyethylene, 3,5-di-tert-butyl-4-hydroxytoluene, 4-benzoyloxy-2, 2,6,6-Tetramethylpiperidine, octadecyl quaternary ammonium sodium and lauric acid are mixed evenly, and the above two mixtures are respectively fed into the extruder from two polyethylene composition feed ports to ...
Embodiment 3
[0173] The method used in this example is similar to the method used in Example 2, the only difference being that the compositions used to prepare three kinds of microporous structure battery separators include the following components by weight:
[0174]
[0175] in,
[0176] The number average molecular weight of high molecular polyethylene is 400,000,
[0177] The number average molecular weight of UHMWPE is 1.4 million.
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