Preparation method for thermal insulation material wet-molded from short-cut carbon fiber
A short-cut carbon fiber and wet forming technology, which is applied in the field of preparing thermal insulation materials, can solve the problems of poor thermal insulation performance, high thermal conductivity, and high production cost, and achieve the effects of low cost, low thermal conductivity, and high material utilization.
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Embodiment 1
[0030] The method for preparing thermal insulation material by wet forming of chopped carbon fiber in this embodiment comprises the following steps:
[0031] (1) Ingredients: chopped polyacrylonitrile-based carbon fiber (10mm long), furan resin (manufacturer: Changshu Dewey Chemical Co., Ltd., FA-2), methylcellulose dispersant (manufacturer: Feicheng Yutian Chemical Co., Ltd. Company, high-grade product) mixed in proportion to obtain the mixture, the mass ratio of the chopped polyacrylonitrile-based carbon fiber to the furan resin = 1: 2, the mass ratio of the methyl cellulose dispersant to the furan resin Mass ratio = 1:100;
[0032] (2) Molding: put the mixture processed in step (1) into a plate-shaped mold with holes, and centrifuge the liquid in the mixture to obtain a semi-moist mixture. The semi-moist mixture is only 25% by weight of the mixture in step (1);
[0033] (3) Curing: Put the mixture and mold processed in step (2) in a curing furnace for curing treatment. Th...
Embodiment 2
[0039] The method for preparing thermal insulation material by wet forming of chopped carbon fiber in this embodiment comprises the following steps:
[0040] (1) Ingredients: chopped viscose-based carbon fiber (0.1mm long), water-based epoxy resin and its curing agent (manufacturer: Shenzhen Heima Chemical Co., Ltd., model: 652, curing agent manufacturer: Shenzhen Heima Chemical Co., Ltd. , model: 536; the dosage of 652: the dosage of 536 is 2:1), Tween dispersant (manufacturer: Wuxi Zhanwang Chemical Reagent Co., Ltd., CAS9005-65-6) and mix uniformly in proportion to obtain the mixture. The mass ratio of chopped viscose-based carbon fiber to the water-based epoxy resin and its curing agent=1: 10, the mass ratio of the Tween dispersant to the water-based epoxy resin and its curing agent=1:10000;
[0041] (2) Forming: Put the mixture processed in step (1) into a cylindrical mold with holes, and vacuum filter and separate the liquid in the mixture to obtain a semi-moist mixture,...
Embodiment 3
[0048] The method for preparing thermal insulation material by wet forming of chopped carbon fiber in this embodiment comprises the following steps:
[0049] (1) Ingredients: Chopped pitch-based carbon fiber (1.0mm long), oily epoxy resin and its curing agent (manufacturer: Shenzhen Heima Chemical Co., Ltd., the amount of resin: the amount of curing agent is 2:1), fluorine Carbon surface active dispersant (manufacturer: Shanghai Jianbang Industrial Co., Ltd., FS-3100) is mixed uniformly in proportion to obtain a mixture, the mass ratio of the chopped pitch-based carbon fiber to the oily epoxy resin and its curing agent = 1:6, the mass ratio of the fluorocarbon surface active dispersant to the oily epoxy resin and its curing agent=1:1000;
[0050] (2) Forming: Put the mixture processed in step (1) into a cylindrical mold with holes, and perform mechanical vibration separation on the liquid in the mixture to obtain a semi-moist mixture. The semi-moist mixture is only For 40% of...
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Abstract
Description
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Application Information

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