Preparation method of palladium nitrate solution
A palladium nitrate solution technology, applied in chemical instruments and methods, ruthenium/rhodium/palladium/osmium/iridium/platinum compounds, inorganic chemistry, etc., can solve the problem of low chloride ion content in palladium nitrate solution, incomplete palladium dissolution, and technical problems The process is difficult to control and other problems, to achieve the effect of shortening the time for nitration, good product consistency, and easy operation
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Embodiment 1
[0019] Take 100 ml of concentrated nitric acid and 400 ml of concentrated hydrochloric acid, and mix them evenly to prepare solvent A.
[0020] 100g of metal palladium powder was weighed and placed in the reactor. The solvent A was added in batches to the reactor equipped with the metal palladium powder. The volume of the solvent A added for the first time was 200ml, and the volume of the solvent A added each time was 100ml. The timing of the addition was after a large amount of yellow gas was not emitted. After heating and dissolving, concentrate the dissolving solution, and when concentrating to 300ml, add concentrated hydrochloric acid to catch the nitrile until no yellow smoke emerges, that is, the nitrification is completed. The reactor was supplemented with deionized water and diluted to 1 L, so that the palladium concentration in the solution was 100 g / L. Add 200ml of reducing agent hydrazine hydrate under stirring state, and the reduction reaction emits a large amount...
Embodiment 2
[0022] Take 300 ml of concentrated nitric acid and 1200 ml of concentrated hydrochloric acid and mix them evenly to prepare solvent A.
[0023] 180 g of metal palladium powder was weighed and placed in the reactor. The solvent A was added in batches to the reactor equipped with the metal palladium powder. The volume of the solvent A added for the first time was 450ml, and the volume of the solvent A added each time was 350ml. The timing of the addition was after a large amount of yellow gas was not emitted. After heating and dissolving, concentrate the dissolving solution, and when concentrating to 600ml, add concentrated hydrochloric acid to catch the nitrile until no yellow smoke emerges, that is, the nitrification is completed. The reactor was supplemented with deionized water and diluted to 1 L, so that the palladium concentration in the solution was 180 g / L. Add 550 ml of reducing agent hydrazine hydrate under stirring, and the reduction reaction emits a large amount of ...
Embodiment 3
[0025] Take 500 ml of concentrated nitric acid and 2000 ml of concentrated hydrochloric acid and mix them evenly to prepare solvent A.
[0026] 250 g of metal palladium powder was weighed and placed in the reactor. The solvent A was added in batches to the reactor equipped with the metal palladium powder. The volume of the solvent A added for the first time was 500ml, and the volume of the solvent A added each time was 500ml. The timing of the addition was after a large amount of yellow gas was not emitted. After heating and dissolving, concentrate the dissolving solution, and when concentrating to 750ml, add concentrated hydrochloric acid to catch the nitrile until no yellow smoke emerges, that is, the nitrification is completed. The reactor was supplemented with deionized water and diluted to 1 L, so that the palladium concentration in the solution was 250 g / L. Add 750ml of reducing agent hydrazine hydrate under stirring, and the reduction reaction emits a large amount of g...
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