Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Organic light-emitting material and application thereof

An electroluminescent material, organic technology, applied in the direction of luminescent materials, organic chemistry, silicon organic compounds, etc., can solve the problems of different, difficult to achieve full-color RGB, efficiency, insufficient life, etc., to achieve the degree of crystallization inhibition, good industrialization The effect of foreground and color purity improvement

Active Publication Date: 2017-02-22
JIANGSU SUNERA TECH CO LTD
View PDF2 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In addition, for the collocation of OLED devices with different structures, the photoelectric functional materials used have strong selectivity, and the performance of the same material in devices with different structures may be completely different.
[0008] At present, the research of fluorescent materials has made great progress and can meet the needs of industrialization; however, there are still deficiencies in its efficiency and lifespan, and it is difficult to meet the requirements of full-color RGB

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Organic light-emitting material and application thereof
  • Organic light-emitting material and application thereof
  • Organic light-emitting material and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0056] Example 1 (compound 06)

[0057] The concrete synthetic route of this compound is provided now:

[0058]

[0059] 250ml four-necked bottle, under the protection of nitrogen, add 0.01mol intermediate A, 0.011mol diphenylamine, 0.03mol sodium tert-butoxide, 1×10 -4 mol Pd 2 (dba) 3 , 1×10 -4 mol tri-tert-butylphosphine, 150ml toluene, heated to reflux for 20 hours, the reaction was complete; naturally cooled, filtered, the filtrate was rotary evaporated, passed through a silica gel column, beaten with a mixed solvent of toluene:ethanol=1:2 (volume ratio), and recrystallized White solid, purity (HPLC) 98.1%, yield 62.2%.

[0060] Elemental analysis structure (molecular formula C 52 h 37 N): theoretical value C, 92.41; H, 5.52; N, 2.07

[0061] Test value: C, 92.39; H, 5.57; N, 2.04

Embodiment 2

[0062] Example 2 (compound 11)

[0063] The concrete synthetic route of this compound is provided now:

[0064]

[0065] In a 250ml four-neck flask, under nitrogen protection, add 0.01mol of intermediate B, 0.011mol of bis(4-tert-butylphenyl)amine, 0.03mol of sodium tert-butoxide, 1×10 -4 mol Pd 2 (dba) 3 , 1×10 -4 mol tri-tert-butylphosphine, 150ml toluene, heated to reflux for 20 hours, the reaction was complete; naturally cooled, filtered, the filtrate was rotary evaporated, passed through a silica gel column, beaten with a mixed solvent of toluene:ethanol=1:3 (volume ratio), and recrystallized White solid, purity (HPLC) 97.8%, yield 60.4%.

[0066] Elemental analysis structure (molecular formula C 50 h 51 N): theoretical value C, 90.18; H, 7.72; N, 2.10

[0067] Test value: C, 89.94; H, 7.76; N, 2.30

Embodiment 3

[0068] Example 3 (compound 15)

[0069] The concrete synthetic route of this compound is provided now:

[0070]

[0071] In a 250ml four-neck flask, under nitrogen protection, add 0.01mol of intermediate C, 0.025mol of bis(4-tert-butylphenyl)amine, 0.03mol of sodium tert-butoxide, 1×10 -4 mol Pd 2 (dba) 3 , 1×10 -4 mol tri-tert-butylphosphine, 150ml toluene, heated to reflux for 20 hours, the reaction was complete; naturally cooled, filtered, the filtrate was rotary evaporated, passed through a silica gel column, beaten with a mixed solvent of toluene:ethanol=1:2.5 (volume ratio), and recrystallized White solid, purity (HPLC) 98.3%, yield 53.1%.

[0072] Elemental analysis structure (molecular formula C 69 h 55 N 2 O): theoretical value C, 89.19; H, 6.07; N, 3.01; O, 1.72

[0073] Test value: C, 89.24; H, 6.10; N, 2.98; O, 1.68

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
thicknessaaaaaaaaaa
thicknessaaaaaaaaaa
thicknessaaaaaaaaaa
Login to View More

Abstract

The invention discloses an organic light-emitting material and application thereof. A structural formula of the light-emitting material is shown as a general formula (1). The material has good fluorescence quantum efficiency and electroluminescence efficiency and has good heat stability. Therefore, the material can be used as a light-emitting layer doped material in an organic electroluminescence device.

Description

technical field [0001] The invention relates to the technical field of semiconductors, in particular to the synthesis of a fluorescent compound and its application in organic light-emitting diodes as a light-emitting layer doping material. Background technique [0002] Organic electroluminescent (OLED: Organic Light Emission Diodes) device technology can be used to manufacture new display products and also can be used to make new lighting products, which is expected to replace the existing liquid crystal display and fluorescent lighting, and has a wide application prospect. [0003] Currently, OLED display technology has been applied in smart phones, tablet computers and other fields, and will further expand to large-size applications such as TVs. However, compared with the actual product application requirements, the luminous efficiency and service life of OLED devices need to be further improved. [0004] The OLED light-emitting device is like a sandwich structure, includ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): C07C211/57C07D307/77C07D307/91C07D333/50C07F7/08C07D209/80C07D209/86C07D405/04C07D409/04C07D405/14C07D409/14C07D219/08C07D265/38C07D279/22C07D413/04C07D319/14C07D407/12C07D311/78C07D411/04C09K11/06H01L51/50H01L51/54
CPCC09K11/06C07C211/57C07D209/80C07D209/86C07D219/08C07D265/38C07D279/22C07D307/77C07D307/91C07D311/78C07D319/14C07D333/50C07D405/04C07D405/14C07D407/12C07D409/04C07D409/14C07D411/04C07D413/04C07F7/0812C09K2211/1025C09K2211/1029C09K2211/1037C09K2211/1033C09K2211/1092C09K2211/1088H10K85/636H10K85/657H10K85/6574H10K85/6576H10K85/6572H10K50/00
Inventor 叶中华李崇张兆超徐凯张小庆
Owner JIANGSU SUNERA TECH CO LTD
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com