Preparation process of sodium sulfide with low content of iron
A low-iron sodium sulfide, manufacturing process technology, applied in the direction of sulfur compounds, alkali metal sulfides/polysulfides, inorganic chemistry, etc., can solve the problem of high iron content in sodium sulfide, reduce impurities, improve quality, iron content volume reduction effect
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Embodiment 1
[0034] The manufacture technology of low-iron sodium sulfide comprises the following steps:
[0035] (1) Use Glauber's salt decahydrate as the raw material for producing sodium sulfide, add Glauber's salt decahydrate to the chemical nitrate tank, and add 80°C distilled water at a ratio of 1:2 to dissolve to form Glauber's salt solution, then put Glauber's salt solution into the evaporator Evaporate in the evaporator, the evaporated liquid enters the crystallization tank for cooling and crystallization, the crystallized Glauber's salt is sent to the centrifuge for centrifugation for 3 minutes, the centrifugal speed of the centrifuge is 1500r / min, and the solid obtained after centrifugation is anhydrous Glauber's salt. The mother liquor obtained after centrifugal separation is returned to the evaporator for recycling;
[0036] (2), crush the anhydrous thenardite prepared in step (1), the particle size after crushing is less than 50mm, then mix the anhydrous thenardite and coal p...
Embodiment 2
[0045] The manufacture technology of low-iron sodium sulfide comprises the following steps:
[0046] (1) Use Glauber's salt decahydrate as the raw material for producing sodium sulfide, add Glauber's salt decahydrate to the chemical nitrate tank, and add 100°C distilled water at a ratio of 1:3 to dissolve to form Glauber's salt solution, then put Glauber's salt solution into the evaporator Evaporate in the evaporator, the evaporated liquid enters the crystallization tank for cooling and crystallization, the crystallized Glauber's salt is sent to the centrifuge for centrifugation for 5 minutes, the centrifugal speed of the centrifuge is 2000r / min, and the solid obtained after centrifugation is anhydrous Glauber's salt. The mother liquor obtained after centrifugal separation is returned to the evaporator for recycling;
[0047] (2), crush the anhydrous thenardite prepared in step (1), the particle size after crushing is less than 50mm, then mix the anhydrous thenardite and coal ...
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