High-Mo Ni3Al-based monocrystal high-temperature alloy modified by rare earth and preparation method of high-Mo Ni3Al-based monocrystal high-temperature alloy
A technology of rare earth modification and high-temperature alloy, which is applied in the field of high-temperature alloys, can solve the problem of unsatisfactory oxidation resistance of alloys, and achieve the effect of improving oxidation resistance
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[0035] The present invention proposes that the rare earth element modified high Mo Ni 3 The Al-based single crystal superalloy is prepared by the following preparation method, which specifically includes the following steps:
[0036] The first step: prepare liquid metal cooling medium; high purity: purity ≥ 99.95%.
[0037] The liquid metal cooling medium is gallium indium alloy or metal tin. The preparation of the gallium-indium alloy: the raw materials of high-purity gallium (Ga) and high-purity indium (In), by weight percentage: gallium 10-30wt%, the rest is indium, weighed, put into a beaker and heat to 80°C ~200°C to make the reaction liquid, pour it into a liquid metal cooling tank as a cooling medium, and use vacuum pump oil to heat around the liquid metal cooling tank to keep the temperature of the cooling tank above 15 °C, so that the gallium-indium alloy remains liquid;
[0038] The preparation of the metal tin: heating the raw material high-purity tin to the melti...
Embodiment 1
[0054] The composition of the alloy in this case is 7.6wt% Al, 9.5wt% Mo, 1.5wt% Re, 3wt% Ta, 1.5wt% Cr, 0.005wt% C, 0.05wt% Y, 0.042wt% Dy, the rest are Ni. The rare earth element modified high Mo Ni 3 The as-cast structure of Al-based single crystal superalloy includes three phase structures of γ′ phase, γ phase and white precipitate phase rich in Mo and Re. The as-cast structure is observed under light microscope and scanning electron microscope as follows figure 1 and figure 2 shown.
[0055] The present invention proposes that the rare earth modified high Mo Ni 3 The Al-based single crystal superalloy is prepared by the following preparation method, which specifically includes the following steps:
[0056] The first step: prepare liquid metal cooling medium; high purity: purity ≥ 99.95%.
[0057] The liquid metal cooling medium is gallium indium alloy or metal tin. The preparation of the gallium-indium alloy: the raw materials high-purity gallium (Ga) and high-puri...
Embodiment 2
[0077] The composition of the alloy in this case is 7wt% Al, 8wt% Mo, 1.5wt% Re, 3wt% Ta, 1.5wt% Cr, 0.001wt% C, 0.01wt% Y, 0.01wt% Dy, The rest is Ni.
[0078] The present invention proposes that the rare earth modified high Mo Ni 3 The Al-based single crystal superalloy is prepared by the following preparation method, which specifically includes the following steps:
[0079] The first step: prepare liquid metal cooling medium; high purity: purity ≥ 99.95%.
[0080] The liquid metal cooling medium is gallium indium alloy or metal tin. The preparation of the gallium-indium alloy: the raw materials high-purity gallium (Ga) and high-purity indium (In), by weight percentage: gallium 10wt%, the rest is indium, weighed, put into a beaker and heated to 80 ° C to make it After the reaction is in a liquid state, pour it into a liquid metal cooling tank as a cooling medium, and use vacuum pump oil to heat around the liquid metal cooling tank to keep the temperature of the cooling ta...
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