Mouthwash powder containing sodium gualenate and preparation method thereof
A technology of sodium azulene sulfonate content, which is applied to medical preparations containing active ingredients, medical preparations with non-active ingredients, oral care, etc., can solve the problems of inconvenient and unstable sodium azulene sulfonate preparations, Achieve good anti-oxidation effect, convenient storage and transportation, and solve the effect of easy oxidation
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Embodiment 1
[0027] A mouthwash powder containing sodium azulene sulfonate, prepared from the following raw materials in terms of mass percentage: 0.4% sodium azulene sulfonate, 0.25% tea polyphenols, 2% sodium bicarbonate, and 94.65% mannitol , Povidone K30 1.5%, Menthol 1%, Flavor 0.2%. Mix the sodium azulene sulfonate and tea polyphenol weighed according to the above amount evenly, mix the obtained mixture with other auxiliary materials by equal addition method, then pass through a 100-mesh sieve twice, mix for 10 minutes, and finally prepare the powder According to 1g / package, it is packed into aluminum-plastic bags.
Embodiment 2~7、 comparative example 1
[0029] Change the amount of tea polyphenols, and simultaneously change the amount of mannitol (see Tables 1-4 for details), and the other raw materials and preparation methods are the same as in Example 1.
[0030] Stability tests were carried out on all the above-mentioned samples, and the test method was as follows.
[0031] The stability test of the present invention is divided into an accelerated test and a long-term test. The accelerated test is to place the sample in a constant temperature and humidity box, store it for 6 months at a temperature of 40°C ± 2°C, and a humidity of 75% ± 5%, and then Take samples at the end of the 0th day and the 1st, 2nd, 3rd, and 6th months, observe the color change and detect the content of sodium azulene sulfonate in the sample, and obtain the proportion of sodium azulene sulfonate in the sample at different times in the initial formula of sodium azulene sulfonate The percentage of dosage, the color change result are shown in Table 1, an...
Embodiment 8
[0046] A mouthwash powder containing azulene sulfonate sodium, prepared from the following raw materials in terms of mass percentage: 0.1% sodium azulene sulfonate, 0.25% tea polyphenols, 2% sodium bicarbonate, and 94.95% mannitol , Povidone K30 1.5%, Menthol 1%, Flavor 0.2%. Mix the sodium azulene sulfonate and tea polyphenol weighed according to the above amount evenly, mix the obtained mixture with other auxiliary materials by equal addition method, then pass through a 100-mesh sieve twice, mix for 10 minutes, and finally prepare the powder According to 1g / package, it is packed into aluminum-plastic bags.
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