High nitrogen resistance hydrocracking catalyst carrier and preparation method thereof
A catalyst carrier and hydrocracking technology, which is applied in the direction of catalyst carrier, physical/chemical process catalyst, molecular sieve catalyst, etc., can solve the problems of poor nitrogen resistance performance, improve nitrogen resistance ability, high cracking activity, and improve anti-sintering ability Effect
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Embodiment 1
[0029] The USY zeolite (purchased from Zibo, Shandong), 40g of amorphous silica-alumina (purchased from Zibo, Shandong) and 20g pseudo-boehmite (purchased from Zibo, Shandong) that are 15 on a dry basis are added to the mixer until uniform, Then add 3g scallop powder, 5g volume ratio 1:1HNO to the mixture 3 solution and 50g of magnesium acetate and lanthanum nitrate mixed solution (containing Mg 0.5g, La 3g), kneading into a dough suitable for extrusion. It was extruded through a die, and the shape was a slender cylinder (diameter 1.7 mm). It was dried at 120°C for 4 hours and then baked at 550°C for 4 hours. Then it was cut into carrier particles of uniform size (1.7×4.0mm) for use.
[0030] The support was impregnated with 3% NiO and 15% MoO by conventional method 3 After sulfide reduction, it is used to investigate the cracking reaction performance. The reaction raw material is 70% toluene + 20% naphthalene + 10% methylnaphthalene, mixed with 95μg / g tert-butylamine, the re...
Embodiment 2
[0032] Beta zeolite (purchased from Zibo, Shandong), 40g amorphous silica-alumina (purchased from Zibo, Shandong) and 20g pseudo-boehmite (purchased from Zibo, Shandong) on a dry basis are added to the mixer until uniform, Then add 3g scallop powder, 5g volume ratio 1:1HNO to the mixture 3 Solution and the mixed solution (containing Mg 0.5g, La3g) of 50g magnesium acetate and lanthanum nitrate, knead into the dough suitable for extruding. It was extruded through a die, and the shape was a slender cylinder (diameter 1.7 mm). It was dried at 120°C for 4 hours and then baked at 550°C for 4 hours. Then it was cut into carrier particles of uniform size (1.7×4.0mm) for use.
[0033] The support was impregnated with 3% NiO and 15% MoO by conventional method 3 After sulfide reduction, it is used to investigate the cracking reaction performance. The reaction raw material is 70% toluene + 20% naphthalene + 10% methylnaphthalene, mixed with 95μg / g tert-butylamine, the reaction tempera...
Embodiment 3
[0035] The dry basis is 20g USY zeolite (purchased from Shandong Zibo) that silicon-aluminum ratio is 15, 20g Beta zeolite (purchased from Shandong Zibo) that silicon-alumina ratio is 15, 40g amorphous silica-alumina (purchased from Shandong Zibo) and 20g Boehmite (purchased from Zibo, Shandong) was added to the mixer until uniform, and then 3g of celadon powder, 5g of HNO in a volume ratio of 1:1 were added to the mixture 3 solution and 50g of magnesium acetate and lanthanum nitrate mixed solution (containing Mg 0.5g, La 3g), kneading into a dough suitable for extrusion. It was extruded through a die, and the shape was a slender cylinder (diameter 1.7 mm). It was dried at 120°C for 4 hours and then baked at 550°C for 4 hours. Then it was cut into carrier particles of uniform size (1.7×4.0mm) for use.
[0036] The support was impregnated with 3% NiO and 15% MoO by conventional method 3 After sulfide reduction, it is used to investigate the cracking reaction performance. The r...
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