Method for preparing conducting film on substrate surface based on silver nanoparticle ink
A technology of silver nanoparticles and the surface of the substrate, which is applied to heat treatment equipment, conductive layers on insulating carriers, circuits, etc., can solve the problems that the nano-conductive film is difficult to meet the process requirements and the production limit of nano-silver TP, and achieve the follow-up The effect of convenient handling, simple and controllable operation process, and cost reduction
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Embodiment 1
[0022] A method for preparing a conductive film on the surface of a substrate based on silver nanoparticle ink, the specific steps are:
[0023] (1) Preparation of silver nanoparticles
[0024] Dissolve silver acetate and octadecylamine in toluene solvent at a molar ratio of 1:5; then take lithium borohydride solution, the molar ratio of lithium borohydride solution to silver acetate is 4:1, add lithium borohydride solution dropwise Add to the mixed solution of silver acetate and octadecylamine, keep stirring during the dropwise addition, the reaction time is 35min, then remove the upper aqueous solution with a separatory funnel, leaving the toluene layer containing silver particles; add ethanol to wash and precipitate nano Particles; Finally, the precipitate is taken out and dried in a vacuum oven at room temperature to obtain a blue dark solid product, which is a solid nano-silver particle;
[0025] (2) Characterization and preparation of silver nanoparticle ink
[0026] T...
Embodiment 2
[0031] A method for preparing a conductive film on the surface of a substrate based on silver nanoparticle ink, the specific steps are:
[0032] (1) Preparation of silver nanoparticles
[0033] Dissolve silver acetate and octadecylamine in toluene solvent at a molar ratio of 1:5; then take lithium borohydride solution, the molar ratio of lithium borohydride solution to silver acetate is 4:1, add lithium borohydride solution dropwise Add to the mixed solution of silver acetate and octadecylamine, keep stirring during the dropwise addition, the reaction time is 40min, then remove the upper aqueous solution with a separatory funnel, leaving the toluene layer containing silver particles; add acetone to wash and precipitate nano Particles; Finally, the precipitate is taken out and dried in a vacuum oven at room temperature to obtain a blue dark solid product, which is a solid nano-silver particle;
[0034] (2) Characterization and preparation of silver nanoparticle ink
[0035] T...
Embodiment 3
[0040] A method for preparing a conductive film on the surface of a substrate based on silver nanoparticle ink, the specific steps are:
[0041] (1) Preparation of silver nanoparticles
[0042] Dissolve silver acetate and octadecylamine in toluene solvent at a molar ratio of 1:5; then take lithium borohydride solution, the molar ratio of lithium borohydride solution to silver acetate is 4:1, add lithium borohydride solution dropwise Add to the mixed solution of silver acetate and octadecylamine, keep stirring during the dropwise addition, the reaction time is 38min, then remove the upper aqueous solution with a separatory funnel, leaving the toluene layer containing silver particles; add ethanol to wash and precipitate nano Particles; Finally, the precipitate is taken out and dried in a vacuum oven at room temperature to obtain a blue dark solid product, which is a solid nano-silver particle;
[0043] (2) Characterization and preparation of silver nanoparticle ink
[0044] T...
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