Application of Cottonone in Preparation of Anti-aging Medicine and Health Food
A technology of cottonone and anti-aging, which is applied in the field of active ingredients of traditional Chinese medicine, and can solve problems such as no reports on anti-aging effects
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Embodiment 1
[0013] The preparation of embodiment 1 Paradone
[0014] Take 1 kg of dried coltsfoot flower and crush it, ultrasonically extract it with petroleum ether for 3 times, each time for 100 min, filter the extract, and concentrate under reduced pressure to obtain 1.23 g of crude extract.
[0015] Take n-hexane, ethyl acetate, methanol, and water (10:5:11:3) in a separatory funnel, let it stand for stratification, the upper phase is the stationary phase, and the lower phase is the mobile phase, and the stationary phase is filled with a pump. Fill the separation column, take the crude extract and dissolve it in the stationary phase to load the sample. When the speed of the main engine reaches 800rpm, pump the mobile phase at a flow rate of 2ml / min. When the mobile phase flows out, collect the target components according to the detector spectrum, concentrate and dry to get coltsfoot Crude ketones. Using petroleum ether-ethyl acetate (35:1) as the eluent, use a silica gel column to se...
Embodiment 2
[0016] Embodiment 2 Paradone anti-aging pharmacodynamics experiment
[0017] 1 material
[0018] 1.1 Model organisms
[0019] Caenorhabditis legans (C.elegans) N2 was kindly provided by Enbo Ma's group at the Institute of Applied Biology, Shanxi University.
[0020] 1.2 Drugs and reagents
[0021] Escherichia coli OP50 (E.coil OP50) was kindly provided by Enbo Ma’s group at the Institute of Applied Biology, Shanxi University, 5-fluoro-2′-deoxyuridine (FUdR) was purchased from sigma (USA), agar powder was purchased from Solarbio (Beijing), peptone was purchased from Beijing Aoboxing Biotechnology Co., Ltd., and other inorganic reagents were purchased from Tianjin Fengchuan Chemical Reagent Co., Ltd. Standard nematode medium NGM medium: each liter medium contains 3g sodium chloride, 21g agar powder, 2.5g peptone, 1mL cholesterol ethanol solution (concentration: 5mg / mL), 1mL CaCl 2 Solution (1mol / L), 1mLMgSO 4 solution (1mol / L) and 25mLKH 2 PO 4 -K 2 HPO 4 Buffer solutio...
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