Polyester film, and transparent electrode film using same
A polyester film and polyurethane technology, applied in the field of polyester film, can solve the problems of reducing screen visibility, visual fatigue, and difficulty in eliminating light interference.
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preparation example 1
[0125] Preparation of the first water dispersion composition for the primer layer
[0126] An adhesive (P3208, Rohm & Haas Company) prepared from 40% by weight methyl methacrylate, 40% by weight ethyl acrylate and 20% by weight melamine was used. 4% by weight of the adhesive, 0.3% by weight of a silicone-based wetting agent (polyester siloxane copolymer, Q2-5212, Dow Corning Corporation), 0.3% by weight of glue with an average particle diameter of 140nm After adding 0.3% by weight of the solid silica particles to water, the mixture was stirred for 2 hours to prepare a first water-dispersed composition. The primer layer prepared by using the first water dispersion composition had a glass transition temperature of 42.4°C, a swelling degree of 29.6%, and a gel ratio of 90.0%.
preparation example 2
[0128] Preparation of the second water dispersion composition for the primer layer
[0129]Add 40 moles (26 mole%) of 2,6-naphthalene dicarboxylic acid (2,6-Naphtalene dicarboxylic acid), 5 moles (3.3 mole%) of sodium 2,5-dicarboxybenzenesulfonate (sodium 2,5- dicarboxylbenzene sulfonate), 5 moles (3.3 mole%) of dimethyl terephthalic acid, 20 moles (13.3 mole%) of bis[(4-(2-hydroxyethoxy)phenyl]fluorene (Bis[4( 2-hydroxyethoxy)phenyl]fluorene), 10 mol (6.6 mol%) of triglyceride (Triglyceride, product of Kao Corporation (trade name: 85P)), 70 mol (46.6 mol%) of ethylene glycol in a solvent-free state After mixing at low temperature, add it into the reactor, raise the temperature by 1°C per minute from 170°C to 250°C and react, remove water or methanol as a by-product, and carry out esterification reaction, while raising the temperature to 260°C, the reaction The pressure in the vessel was reduced to 1 mm Hg, the diol was recovered as a by-product, and the polycondensation re...
preparation example 3
[0132] Preparation of the third water dispersion composition for the primer layer
[0133] A water-dispersible polyurethane having a theoretical branched polyol content of 50% by weight was prepared. By making 40% by weight of polyol (Polyethyleneadipate Diol: polyethylene adipate diol), 0.6% by weight of trimethylol propane (Trimethylol Propane), 55.9% by weight of hexamethylene diisocyanate (hexamethylenediisocyanate) ) reaction, after preparing the prepolymer (Prepolymer) with the isocyanate functional group as the terminal group, as an ionic group, 3.5% by weight of sodium hydrogen sulfate (Sodium Hydrogen Sulfate) is reacted with the isocyanate as the terminal functional group of the prepolymer to prepare Polyurethane with ionic groups and a weight-average molecular weight of 14400 g / mol.
[0134] The prepared 20% by weight polyurethane was dispersed in 80% by weight water to prepare a polyurethane adhesive with a solid content of 20% by weight. The 4% by weight of th...
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