A kind of mullite lightweight heat insulation brick and preparation method thereof

A lightweight heat insulation and mullite technology, which is applied in ceramic products, other household utensils, household utensils, etc., can solve the problems of low compressive strength and bulk density, high thermal conductivity of products, and large line change rate after firing. Achieve the effects of low linear shrinkage, good thermal stability and low bulk density

Active Publication Date: 2020-02-14
WUHAN UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although the manufactured product has high compressive strength, its defects are: complex preparation process, high thermal conductivity of the product, and high linear shrinkage
[0004] "A clay lightweight brick and its preparation method" (CN103435332A) patented technology, the patented technology uses 30~40wt% kyanite or coke gem, 35~45wt% fly ash and 15~35wt% plastic clay As a raw material, add 35~55wt% pore forming agent or 2~4wt% polystyrene balls of the raw material, and add 6~10wt% binder of the raw material, mix well, granulate, and then pass the semi-dry method Lightweight insulation bricks are prepared by vibration and pressure molding. Although the products produced have high compressive strength and low bulk density, the disadvantages are: complex preparation process and large line change rate after firing
Although the manufactured products have low bulk density and high compressive strength, the disadvantages are that the line change rate after firing is too large and the thermal conductivity is too large

Method used

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Experimental program
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Effect test

preparation example Construction

[0029] The preparation method of the described pore-forming agent is: according to sawdust: the mass ratio of silica sol is (1.5~2): 1, adds silica sol to sawdust, stirs evenly, in 10 3 ~10 4 Immerse 5~10min under Pa condition, dry, obtain modified sawdust; Then described primary modified sawdust is ball milled 3~5h, after ball milling, modified sawdust is at 10 3 ~10 4Pa stand for 2 to 3 minutes, and dry to obtain a pore-forming agent.

[0030] The main chemical composition of the kyanite is: SiO 2 35~40wt%, Al 2 o 3 55~60wt%, ZrO 2 1~2wt%, Fe 2 o 3 0.5~0.9wt%, CaO+MgO 0.5~0.8wt%, loss on ignition 0.1~0.25wt%; the particle size of kyanite is less than 0.088mm.

[0031] The main chemical composition of the burnt gem is: Al 2 o 3 45~50wt%, SiO 2 40~50wt%, Fe 2 o 3 0.5~1wt%, CaO 0.5~0.6wt%, MgO 0.2~0.3wt%, Na 2 O is 0.5~1.0wt%, K 2 O is 0.1-0.2wt%, loss on ignition is 1-1.5wt%; the particle size of the burnt gem is less than 0.088mm.

[0032] The α-Al 2 o 3 The...

Embodiment 1

[0037] A mullite lightweight heat-insulating brick and a preparation method thereof. The raw materials and contents of the mullite lightweight heat-insulating bricks are: 40-44wt% of coke gem, 33-38wt% of kyanite, 6-12wt% of clay, α-Al 2 o 3 The micro powder is 14-20wt%; the binder is 19-20wt% of the raw material, and the pore-forming agent is 45-48wt% of the raw material.

[0038] The preparation method of the mullite lightweight heat-insulating brick is: according to the content of the above-mentioned raw materials, binder and pore-forming agent, the α-Al 2 o 3 Mix micropowder with pore-forming agent, wet mill for 8-10 hours to obtain homogeneous mud, then stir the homogeneous mud, burnt gemstone, kyanite, clay and binder at room temperature for 6-10 hours, trap materials, and form , baked at 110°C for 24 hours, and kept at 1325-1350°C for 3-5 hours to obtain mullite lightweight heat-insulating bricks.

[0039] In this embodiment: the clay is Suzhou soil; the binder is p...

Embodiment 2

[0042] A mullite lightweight heat-insulating brick and a preparation method thereof. The raw materials and contents of the mullite lightweight heat-insulating bricks are: 41~45wt% of coke gemstone, 28~33wt% of kyanite, 7~13wt% of clay, α-Al 2 o 3 The micro powder is 15-21wt%; the binder is 18-19wt% of the raw material, and the pore-forming agent is 48-51wt% of the raw material.

[0043] The preparation method of the mullite lightweight heat-insulating brick is: according to the content of the above-mentioned raw materials, binder and pore-forming agent, the α-Al 2 o 3 Mix micropowder with pore-forming agent, wet mill for 8-10 hours to obtain homogeneous mud, then stir the homogeneous mud, burnt gemstone, kyanite, clay and binder at room temperature for 6-10 hours, trap materials, and form , baked at 110°C for 24 hours, and kept at 1350-1375°C for 3-5 hours to obtain mullite lightweight heat-insulating bricks.

[0044] In this embodiment: the clay is kaolin; the binder is a...

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Abstract

The invention specifically relates to a mullite lightweight heat-insulating brick and a preparation method thereof. The technical solution is: the raw material and content of the mullite lightweight heat-insulating brick are: 40-48wt% of coke gemstone, 14-38wt% of kyanite, 6-16wt% of clay, α-Al 2 o 3 The micro powder is 14-24wt%; the binder is 15-20wt% of the raw material, and the pore-forming agent is 45-60wt% of the raw material. According to the content of the above-mentioned raw materials, binders and pore-forming agents, the α-Al 2 o 3 Mix micropowder with pore-forming agent, wet mill for 8-10 hours to obtain homogeneous mud; then stir homogeneous mud, burnt gemstone, kyanite, clay and binder evenly, trap material, shape, bake, Keep warm for 3~5h under the condition of ℃ to get mullite lightweight insulation brick. The invention saves resources, has a simple process and is environmentally friendly, and the prepared mullite lightweight heat-insulating brick has good thermal stability, low thermal conductivity, small bulk density, low linear shrinkage after firing, high compressive strength and heat insulation. The effect is good.

Description

technical field [0001] The invention belongs to the technical field of lightweight heat insulating bricks. It specifically relates to a mullite lightweight heat-insulating brick and a preparation method thereof. Background technique [0002] At present, affected by the lack of energy at home and abroad and the price of available energy, the development of new energy-saving refractory materials has a huge market demand at home and abroad. The research and development of environmentally friendly heat-insulating refractory materials and the preparation of low-density, low thermal conductivity, high-strength, and low-cost lightweight heat-insulating materials have become the mainstream direction. [0003] "A high-silicon mullite with the structure of gramineous plants and its preparation method" (CN201410457026.9) patent technology, using 30~90wt% aluminum sol as impregnating agent in normal pressure or 10 3 ~10 4 Soaking under Pa conditions, stirring evenly; then baking the ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B35/66C04B35/185C04B38/06
CPCC04B35/185C04B35/66C04B38/0675C04B2235/3217C04B2235/3418C04B2235/3427C04B2235/3463C04B2235/349C04B2235/77C04B2235/96C04B2235/9607C04B2235/9615C04B38/0067
Inventor 李远兵刘建博李淑静向若飞徐娜娜欧阳思
Owner WUHAN UNIV OF SCI & TECH
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