A kind of graphite sealing material and preparation method thereof
A graphite sealing and graphite technology, applied in chemical instruments and methods, other chemical processes, etc., can solve the problems of continuous or intermittent high temperature, muon pressure, muon corrosion, prestressing stress, seal failure, limitation and so on
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[0063] The present invention also provides a kind of preparation method of graphite sealing material, comprises the following steps:
[0064] 1) After mixing fibers, rubber, rubber additives, non-asbestos fibers and fillers, a masterbatch is obtained;
[0065] 2) Rolling and vulcanizing the masterbatch obtained in the above steps to obtain a sealing material.
[0066] The selection and optimization principles of raw materials in the above preparation method in the present invention can correspond to the selection and optimization principles of raw materials in the aforementioned graphite sealing material, and will not be repeated here.
[0067] The present invention has no special restrictions on the pretreatment process of rubber in the preparation process, and the rubber pretreatment steps well known to those skilled in the art can be used. Those skilled in the art can select and adjust according to actual production conditions, product quality and use requirements. , the r...
Embodiment 1
[0098] Refer to Table 1 for the production formula of graphite sealing liner plate type I.
[0099] Table 1
[0100] Thickness: 0.25~3.00mm
Graphite sealing liner plate type I
Raw material name
Actual dosage (kg)
Nitrile rubber
28.00
total
28.00
sulfur powder
0.96
Accelerator
0.90
Zinc oxide
1.80
plasticizer
0.50
Antiaging agent
0.80
total
4.96
Silica
10.00
Kaolin
13.00
graphite powder
45.00
Man-made mineral fiber
44.00
Aramid pulp
10
total
122.00
total
154.96
toluene
85L
Alcohol
22L
[0101] Preparation steps:
[0102] Process 1: Mastication of nitrile rubber
[0103] According to the dosage specified in the formula, weigh the nitrile rubber (tolerance ± 0.2kg);
[0104] The weighed nitrile rubber is masticated twice on a rubber mixing machine wi...
Embodiment 2
[0135] Refer to Table 3 for the production formula of graphite sealing backing plate Type II.
[0136] table 3
[0137] Thickness: 0.25~3.00mm
Graphite sealing backing plate type II
Raw material name
Actual dosage (kg)
Hydrogenated nitrile rubber
32.00
total
32.00
sulfur powder
1.11
Accelerator
0.94
Zinc oxide
1.50
plasticizer
0.90
Antiaging agent
0.60
total
5.05
Silica
12.00
carbon black
5.00
graphite powder
50.00
Man-made mineral fiber
36.00
Aramid pulp
15.00
total
118.00
total
155.05
toluene
98L
Alcohol
43L
[0138] Preparation steps:
[0139] Process 1: mastication of hydrogenated nitrile rubber
[0140] Weigh the hydrogenated nitrile rubber (tolerance ± 0.2kg) according to the dosage specified in the formula;
[0141] The weighed hydrogenated...
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