Polycarbonate insulating heat-conducting composite material and preparation method thereof
A composite material, insulation and heat conduction technology, which is applied in the field of coating production, can solve the problems that high thermal conductivity composite materials cannot meet the requirements of low dielectric coefficient and electrical insulation performance, and achieve excellent electrical insulation performance and improve thermal conductivity.
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Embodiment 1
[0020] A preparation method of polycarbonate insulating and thermally conductive composite material includes the following steps:
[0021] (1) Dissolve 12-15g of N-β(aminoethyl)-γ-aminopropylmethyldimethoxysilane silane coupling agent in 100ml of 95% ethanol solution and ultrasonically disperse into 12-15wt% silane coupling Coupling agent-water solution;
[0022] (2) The silane coupling agent-water solution is sprayed into the insulating and thermally conductive composite material. The insulating and thermally conductive composite material is a composite composed of 24-25g epoxy resin and 4-12g polycarbonate. The temperature is increased to 85-120℃ , Stir for 1-2 hours, cool for later use;
[0023] (3) Mix 12-15g of reinforced matrix material and 0.4-3g of other functional additives for no less than 30 minutes. The reinforced matrix is a mixture of glass fiber, chopped carbon fiber and hexagonal boron carbide. Agents include anti-aging agents, plasticizers, flame retardants, acti...
Embodiment 2
[0027] A preparation method of polycarbonate insulating and thermally conductive composite material includes the following steps:
[0028] (1) Dissolve 12-15g of γ-aminopropylmethyldimethoxysilane in 100ml of 95% ethanol solution, and ultrasonically disperse into 12-15wt% silane coupling agent-water solution;
[0029] (2) The silane coupling agent-water solution is sprayed into the insulating and thermally conductive composite material. The insulating and thermally conductive composite material is a composite composed of 24-25g epoxy resin and 4-12g polycarbonate. The temperature is increased to 85-120℃ , Stir for 1-2 hours, cool for later use;
[0030] (3) Mix 12-15g of reinforced matrix material and 0.4-3g of other functional additives for no less than 30 minutes. The reinforced matrix is a mixture of glass fiber, chopped carbon fiber and hexagonal boron carbide. Agents include anti-aging agents, plasticizers, flame retardants, active zinc oxide, aromatic salicylate, dibutyl tin...
Embodiment 3
[0034] A preparation method of polycarbonate insulating and thermally conductive composite material includes the following steps:
[0035] (1) Dissolve 15g of γ-aminopropylmethyldiethoxysilane in 100ml of 95% ethanol solution and ultrasonically disperse into 15wt% silane coupling agent-water solution;
[0036] (2) The silane coupling agent-water solution is sprayed into the insulating and thermally conductive composite material. The insulating and thermally conductive composite material is a composite composed of 24g epoxy resin and 12g polycarbonate. The temperature is increased to 85-120°C, and stirred 1- 2 hours, cool for later use;
[0037] (3) Mix 12g of reinforced matrix material and 3g of other functional additives for no less than 30 minutes. The reinforced matrix is a mixture of glass fiber, chopped carbon fiber and sphalerite-type boron carbide. The remaining functional additives include anti- Aging agent, plasticizer, flame retardant, active zinc oxide, aromatic salicyl...
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