Special lubricating grease for numerically-controlled machine tools and preparation method of special lubricating grease
A technology of CNC machine tools and grease, applied in the field of special grease, which can solve the problem of large friction resistance of grease lubrication
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Embodiment 1
[0015] (1) Add 12 kg of thickener and 35 kg of base oil into the saponification kettle, heat up until the thickener melts and start stirring, wherein the thickener consists of 8.4 kg of stearic acid and 3.6 kg of lauryl hydroxystearic acid , the base oil is a mixture of mineral oil and synthetic lubricating oil;
[0016] (2) Dissolve 5 kg of lithium hydroxide in water to form an aqueous solution of lithium hydroxide. When the temperature of the mixed solution in step (1) rises to 65°C, add the aqueous solution of lithium hydroxide to the saponification kettle, and continue to saponify at 105 Saponification at ℃ for 3h;
[0017] (3) After the saponification reaction is completed, continue to stir and raise the temperature for dehydration. When the temperature reaches 155°C, take a sample to measure the free base of the soap base. After the material is qualified, continue to heat up to 195°C and add 35 kg of base oil for thickening. The base oil is mineral oil and Synthesize th...
Embodiment 2
[0020] (1) Add 10 kg of thickener and 25 kg of base oil into the saponification kettle, heat up until the thickener melts, and then start stirring. The thickener consists of 8.5 kg of stearic acid and 1.5 kg of lauryl hydroxystearic acid , the base oil is a mixture of mineral oil and synthetic lubricating oil;
[0021] (2) Dissolve 3 kg of lithium hydroxide in water to form an aqueous solution of lithium hydroxide. When the temperature of the mixed solution in step (1) rises to 60°C, add the aqueous solution of lithium hydroxide to the saponification kettle, and continue to saponify at 100 Saponification at ℃ for 3h;
[0022] (3) After the saponification reaction is completed, continue to stir and raise the temperature for dehydration. When the temperature reaches 150°C, take a sample to measure the free base of soap base. After passing the material, continue to heat up to 190°C and add 35 kg of base oil for thickening. The base oil is mineral oil and Synthesize the mixture o...
Embodiment 3
[0025] (1) Add 15 kg of thickener and 45 kg of base oil into the saponification kettle, heat up until the thickener melts, and then start stirring. The thickener is composed of 12 kg of stearic acid and 3 kg of lauryl hydroxystearic acid , the base oil is a mixture of mineral oil and synthetic lubricating oil;
[0026] (2) Dissolve 8 kg of lithium hydroxide in water to form an aqueous solution of lithium hydroxide. When the temperature of the mixed solution in step (1) rises to 70°C, add the aqueous solution of lithium hydroxide to the saponification kettle, and continue to saponify at 110 Saponification at ℃ for 3h;
[0027] (3) After the saponification reaction is completed, continue to stir and heat up for dehydration. When the temperature reaches 160°C, take a sample to measure the free base of soap base. After passing the material, continue to heat up to 200°C and add 40 kg of base oil to thicken. The base oil is mineral oil and Synthesize the mixture of lubricating oil,...
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