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Environment friendly quenching agent used for abrasion-resistant alloy machining and preparation method thereof

A wear-resistant alloy and environment-friendly technology, applied in the field of materials, can solve problems such as accelerated aging, quality reduction of heat-treated products, and changes in cooling characteristics, and achieve the effect of improving the wear resistance of alloys

Inactive Publication Date: 2017-05-31
HENAN TIMECLOUD COMM TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In use, the organic solution will accelerate aging after being heated, and its cooling characteristics will change. If it is not replaced in time, the quality of the heat-treated product will be reduced, or even unqualified.
At present, there is no uniform quenching agent for the quenching treatment of wear-resistant material workpieces in the market. The quenching treatment process of wear-resistant materials is an important part of the toughness of the workpiece. It is necessary to develop wear-resistant material quenching agents.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] An environment-friendly quenching agent for wear-resistant alloy processing, characterized in that, in parts by weight, it consists of the following raw materials: 5 parts of ethanol, 2 parts of acetate, 0.5 parts of stearic acid, 7 parts of sodium sulfate, potassium hydroxide 2 parts, 15 parts of sweet potato starch, 3 parts of 6-acetoxymethyl-2,2-dimethyl-1,3-dioxolane-tert-butyl acetate, 5 parts of D-aspartic acid, palm oil 10 parts, 8 parts of polyethylene glycol.

[0019] A preparation method of an environment-friendly quenching agent for wear-resistant alloy processing, the specific steps are:

[0020] (1) First, dissolve stearic acid, sweet potato starch, and palm oil in ethanol to obtain a mixed solution, then add water three times the volume of the mixed solution and transfer it to a reactor. The reaction conditions are 140°C, 800r / min, 2MPa , the reaction time is 1h, after the reaction is finished, the temperature drops to 80°C, and acetate and 6-acetoxymethy...

Embodiment 2

[0023] An environment-friendly quenching agent for wear-resistant alloy processing, characterized in that, in parts by weight, it consists of the following raw materials: 8 parts of ethanol, 4 parts of acetate, 0.8 parts of stearic acid, 8 parts of sodium sulfate, potassium hydroxide 2 parts, 18 parts of sweet potato starch, 3 parts of 6-acetoxymethyl-2,2-dimethyl-1,3-dioxolane-tert-butyl acetate, 5 parts of D-aspartic acid, palm oil 14 parts, 8 parts of polyethylene glycol.

[0024] A preparation method of an environment-friendly quenching agent for wear-resistant alloy processing, the specific steps are:

[0025] (1) First, dissolve stearic acid, sweet potato starch, and palm oil in ethanol to obtain a mixed solution, then add water three times the volume of the mixed solution and transfer it to a reactor. The reaction conditions are 145°C, 800r / min, 2MPa , the reaction time is 1h, after the reaction is completed, the temperature drops to 83°C, and acetate and 6-acetoxymeth...

Embodiment 3

[0028] An environment-friendly quenching agent for wear-resistant alloy processing, characterized in that, in parts by weight, it consists of the following raw materials: 10 parts of ethanol, 5 parts of acetate, 0.9 parts of stearic acid, 9 parts of sodium sulfate, potassium hydroxide 3 parts, 21 parts of sweet potato starch, 6 parts of 6-acetoxymethyl-2,2-dimethyl-1,3-dioxolane-tert-butyl acetate, 8 parts of D-aspartic acid, palm oil 16 parts, 10 parts of polyethylene glycol.

[0029] A preparation method of an environment-friendly quenching agent for wear-resistant alloy processing, the specific steps are:

[0030] (1) First, dissolve stearic acid, sweet potato starch, and palm oil in ethanol to obtain a mixed solution, then add water three times the volume of the mixed solution and transfer it to the reactor. The reaction conditions are 147°C, 900r / min, 2.5 MPa, the reaction time is 1.5h, after the reaction is finished, the temperature drops to 85°C, add acetate and 6-acet...

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PUM

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Abstract

The invention discloses an environment friendly quenching agent used for abrasion-resistant alloy machining. The environment friendly quenching agent used for abrasion-resistant alloy machining is composed of the following raw materials including, by weight, 5-13 parts of ethyl alcohol, 2-7 parts of acetic acid ester, 0.5-1.4 parts of stearic acid, 7-10 parts of sodium sulfate, 2-4 parts of potassium hydroxide, 15-26 parts of sweet potato starch, 3-8 parts of 6-acetyl oxygen methyl-2,2-dimethyl-1,2-dioxolame-tert-butyl acetate, 5-10 parts of D-aspartic acid, 10-17 parts of palm oil and 8-12 parts of polyethylene glycol. The stearic acid, the sweet potato starch and the palm oil are dissolved in ethyl alcohol firstly, and a mixed solution is obtained; then the mixed solution is added with water and transferred into a reaction still; after the reaction is finished, temperature reduction is conducted, the acetic acid ester and the 6-acetyl oxygen methyl-2,2-dimethyl-1,2-dioxolame-tert-butyl acetate are added, and still standing is conducted after stirring; then centrifugation is conducted, and a liquid supernatant is taken after centrifugation; and the sodium sulfate, the potassium hydroxide, the D-aspartic acid and the polyethylene glycol are added, temperature rising, thermal insulation, temperature reduction and mouth sealing through paraffin oil are conducted after even stirring, and the environment friendly quenching agent is obtained. The prepared environment friendly quenching agent used for abrasion-resistant alloy machining can greatly improve abrasive resistance of alloys.

Description

technical field [0001] The invention relates to the technical field of materials, in particular to an environment-friendly quenching agent for wear-resistant alloy processing. Background technique [0002] Quenching agent is a process oil used as a quenching medium. The quenching agent must have the following characteristics: good cooling performance, high flash point and ignition point, good thermal oxidation stability, low viscosity, and low moisture content. In addition to the above characteristics, the quenching agent should also be non-toxic, odorless, easy to handle, non-polluting to the environment, and make the surface of the quenched workpiece bright. According to the cooling rate, it can be divided into: (1) ordinary quenching agent; (2) fast quenching agent; (3) super (high) speed quenching agent. Ultrafast quenching agents have a fairly fast cooling rate, faster than rapid quenching agents. The oil is prepared by adding refrigerant, detergent and antioxidant t...

Claims

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Application Information

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IPC IPC(8): C21D1/58
CPCC21D1/58
Inventor 不公告发明人
Owner HENAN TIMECLOUD COMM TECH CO LTD
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