A kind of high temperature resistant lithium ion battery separator and preparation method thereof
A technology for lithium ion batteries and battery separators, applied in battery pack components, circuits, electrical components, etc., can solve problems such as restricting the development of lithium ion batteries, low lithium ion conductivity, and increasing battery impedance, and achieve consistent voltage and quality. High, shrinkage reduction effect
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[0044] ①Al 2 o 3 Preparation of coating slurry:
[0045] Add N-methylpyrrolidone and aluminum oxide powder to a vacuum, high-speed, planetary stirring device with ultrasonic oscillation function at the same time. h, to obtain slurry;
[0046] Add one or more mixtures of sodium polyacrylate, sodium polymetaphosphate, sodium orthophosphate, sodium silicate, sodium lauryl sulfate, and ammonia water to the slurry in an amount of 0.5% of the slurry; Add static eliminator, the addition amount is 0.3% of the slurry, high-speed stirring and ultrasonic oscillation for 0.5h;
[0047] Add one or more mixtures of alcohol, propylene carbonate, glycerin, dimethyl sulfoxide, polyoxyethylene alkylphenol ether, polyoxyethylene fatty alcohol ether, polyvinyl alcohol, and the amount added is the slurry 0.5%; high-speed stirring and ultrasonic oscillation for 0.5h;
[0048] Add PVDF glue with a slurry amount of 5%, and sodium carboxymethylcellulose with a slurry amount of 0.3%; high-speed st...
Embodiment 1
[0085] Take a 16um wet-process PE separator, select one side of the wet-process PE separator and use a micro-gravure roller to coat 2um thick Al 2 o 3 Apply the slurry to form a coating film, and then use a dipping coating device to coat 1um oily SiO on both sides of the coating film 2 Coating the slurry to obtain Al with a thickness of 20 μm 2 o 3 and SiO 2 Two kinds of slurry-coated composite Li-ion battery separators with a structure of SiO 2 Coating-Al 2 o 3 Coating-PE Separator-SiO 2 coating.
[0086] The preferred preparation method of the lithium-ion battery diaphragm in this embodiment is:
[0087] A. Preparation of coating slurry: preparation of Al 2 o 3 Coating paste and SiO 2 Coating slurry, standby;
[0088] B. Pretreatment of battery diaphragm: Use ozone with a flow rate of 0.5L / min to pretreat the diaphragm for 120s, and reserve it; if the pretreatment time is too short, it will affect the surface adhesion of the diaphragm and the appearance quality o...
Embodiment 2
[0092] Take a 10um wet-process PP diaphragm, and coat 2um-thick SiO on both sides of the wet-process PP diaphragm with a dip coating device 2 Apply the slurry to form a coating film, and then use a dip coating device to coat 1um oily Al on both sides of the coating film 2 o 3 Coating the slurry to obtain SiO with a thickness of 16 μm 2 and Al 2 o 3 Two kinds of slurry-coated composite Li-ion battery separators with a structure of Al 2 o 3 Coating - SiO 2 Coating - PP Separator - SiO 2 Coating-Al 2 o 3 coating.
[0093] The preferred preparation method of the lithium-ion battery diaphragm in this embodiment is:
[0094] A. Preparation of coating slurry: preparation of Al 2 o 3 Coating paste and SiO 2 Coating slurry;
[0095] B. Pretreatment of battery diaphragm: use ozone with a flow rate of 1L / min to pretreat the diaphragm for 100s, and reserve it; if the pretreatment time is too short, it will affect the surface adhesion of the diaphragm and the appearance quali...
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