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Ginkgo testa pectin extraction method

A technology for extracting ginkgo testa and pectin, which is applied in the field of food and medicine, can solve the problems of microbial activity and fermentation conditions, limitations that cannot meet production needs, and unstable product quality, etc., to reduce energy consumption, Improve the yield of pectin extraction and the effect of increasing the yield

Inactive Publication Date: 2017-06-09
DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Traditional pectin extraction methods include boiling water extraction, acid hydrolysis, microbial method, microwave-assisted extraction, etc. These extraction methods have certain limitations and cannot meet production needs
For example, the pectin extracted by the boiling water extraction method and the acid hydrolysis method has a darker color; the microbial method is greatly affected by the activity of the strain and fermentation conditions, and the product quality is unstable; although the pectin obtained by the microwave method is of high quality, it is difficult to scale up Cannot be used in industrial production

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039] A kind of Ginkgo biloba testa pectin extracting method provided by the invention, comprises the following steps successively:

[0040] (1) Picking of ginkgo fruit

[0041] Choose to pick during the green fruit period (July-September) of Ginkgo biloba, store in a ventilated environment; peel off the outer testa for later use.

[0042] (2) Ginkgo biloba testa pretreatment

[0043] Weigh 1000 grams of Ginkgo biloba testa, filter and remove moldy and corrupt raw materials, wash the selected raw materials 3 times to remove impurities such as soil, sand, iron filings, etc., air shower for 10 minutes, and use a food grinder to grind the raw materials smash. (3) Pectin extraction

[0044] Add leaching solution to the pulverized raw material in a ratio of 1:10 by mass, and the leaching solution consists of: sodium phosphate (Na 3 PO 4 )3%, disodium hydrogen phosphate (Na 2 HPO 4 ) 0.9%, sodium citrate (Na 3 C 6 h 5 o 7 ) 50mM, glycolic acid (HOCH 2 COOH) 0.4%. Adjust ...

Embodiment 2

[0090] A kind of Ginkgo biloba testa pectin extracting method provided by the invention comprises the following steps successively:

[0091] (1) Picking of ginkgo fruit

[0092] Choose to pick the ginkgo at the green fruit stage, store it in a ventilated environment, and keep it for later use.

[0093] (2) Ginkgo biloba testa pretreatment

[0094] Weigh 1000 grams of Ginkgo biloba testa, filter and remove moldy and corrupt raw materials, wash the selected raw materials 3 times to remove impurities such as soil, sand, iron filings, etc., air shower for 10 minutes, and use a food grinder to grind the raw materials smash.

[0095] (3) Pectin extraction

[0096] Add leaching solution to the pulverized raw material in a ratio of 1:10 by mass, and the leaching solution consists of: sodium phosphate (Na 3 PO 4 ) 8%, disodium hydrogen phosphate (Na 2 HPO 4 ) 1.5%, sodium citrate (Na 3 C 6 h 5 o 7 ) 100mM, glycolic acid (HOCH 2 COOH) 1%. Adjust the pH value to 2 with hydro...

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PUM

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Abstract

The invention discloses a ginkgo testa pectin extraction method, and aims to provide a novel ginkgo testa pectin extraction method which has the advantages of high product quality and high extraction yield and can implement industrial production. The technical scheme is as follows: the method comprises the following steps: (1) picking ginkgos in the green fruit period (July-September); (2) flushing the ginkgo testae three times, and mashing with a food pulverizer; (3) extracting the mashed ginkgo testae in an extracting solution for 45-120 minutes to obtain pectin; (4) decolorizing the extracted pectin solution with activated carbon; (5) concentrating the decolorized pectin solution through a ceramic ultrafiltration membrane, wherein the concentration percent is 20-50 vol% of the original solution; (6) precipitating the concentrated pectin solution with ethanol; (7) purifying the pectin crude extract by ethanol soaking; and (8) drying the purified pectin at 50-70 DEG C, and pulverizing to obtain pectin powder.

Description

technical field [0001] The technology relates to the field of food and medicine, in particular to a method for extracting ginkgo exocarp pectin. Background technique [0002] Pectin is a natural polysaccharide polymer with a molecular weight between 50,000 and 300,000. The main chain is a long chain structure of D-galacturonic acid connected by α-1,4 glycosidic bonds. The side chain is composed of A short chain structure composed of rhamnose, arabinose, galactose and xylose. Pectin is white to yellow-brown powder, colorless, odorless, without fixed melting point and solubility, insoluble in organic solvents such as ethanol, but soluble in hot water and slightly soluble in cold water. Pectin is the main component of dietary fiber, the seventh largest nutrient in the human body. It has a variety of edible and medicinal values, so it has a wide range of applications in food, medicine and other fields. In the field of food, pectin is often used as gelling agent, thickener, sta...

Claims

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Application Information

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IPC IPC(8): C08B37/06
Inventor 孙广炜张英吕国军刘洋赵姗
Owner DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI
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