Pharmaceutical composition for treating migraine
A composition and technology for migraine, applied in the directions of drug combination, pharmaceutical formula, pill delivery, etc., can solve problems such as addiction, mental and physical dependence, and achieve the effects of improving symptoms, being convenient to carry, and having good preventive and therapeutic effects.
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Embodiment 1
[0043] 1. Preparation of Armillaria polysaccharide
[0044] 1.1 Preparation of Armillaria fruiting body polysaccharide: Weigh Armillaria fruiting body according to 20 times of the above mass ratio, wash and dry at 60°C, crush into a coarse powder of about 1 mm, the ratio of solid to liquid is 1:20, and the temperature is 100°C. Add water and reflux to extract twice, the first time is 3 hours, and the second time is 2 hours; combine the extracts and concentrate in vacuum to form a clear paste with a relative density of 1.10-1.20 (room temperature); use 3-4 times the amount of 95% ( mass fraction) ethanol precipitation for 24 hours; take the precipitate, wash it with absolute ethanol 3 times, then dissolve it with 4 times the amount (mass fraction) of ≥80°C hot water, let it cool to 40°C~50°C, add 1%~ 3% (mass ratio) papain, keep warm for 4 to 5 hours; add chloroform / n-butanol mixed solution according to the ratio of polysaccharide aqueous solution: chloroform: n-butanol 25:4:1...
Embodiment 2
[0047] Preparation of low-molecular-weight fucoidan sulfate: take fucoidan sulfate extracted from kelp or fucus, dissolve it in water at a ratio of 1.5% to 3.0%, and sterilize at 100°C for 20-30min; cool the aqueous solution of fucoidan sulfate to 60°C- At 70°C, add arabinofuranosidase at a ratio of 1% to 3%, the optimum pH is ≤7, the optimum reaction temperature is 60°C, and the reaction time is 4 to 5 hours to degrade fucoidan sulfate; vacuum concentration, concentrated solution Add ethanol to 75%, collect the precipitate, dry and pulverize to obtain low molecular weight fucoidan sulfate ester, and its molecular weight (MW) should be 60,000-130,000.
Embodiment 3
[0049] Preparation of the active composition granules of the present invention: Weigh 1000g of Armillaria polysaccharide, 100g of low molecular weight fucoidan sulfate, 250g of γ-aminobutyric acid, and 1650g of maltodextrin, mix them evenly, and use a 14-16 mesh nylon sieve Made into wet granules, dried at 50°C to 60°C until the moisture content is ≤5.0% (mass ratio), packed into bags, 3g per bag, made into 1000 bags.
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