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Printing adhesive and preparation method thereof, printing paste and clothing

An adhesive and printing technology, applied in the field of light industrial textiles, can solve the problems of limited performance improvement and environmental protection, and achieve the effect of clear flower shape, low environmental pollution and stable storage

Inactive Publication Date: 2017-07-28
XIAMEN ANTA SPORTS GOODS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] The invention provides a printing adhesive and its preparation method to solve the problems of limited performance improvement and environmental protection in the prior art

Method used

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  • Printing adhesive and preparation method thereof, printing paste and clothing

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0073] Heat up 40.0g of cooling silicone oil emulsion SOFTEXS-585, 0.6g of emulsifier, and 60g of deionized water to 40°C, and stir evenly for 2 hours to obtain the first component; 30.0g of butyl acrylate, 20.0g of isooctyl acrylate, Methyl methacrylate 10.0g, acrylonitrile 5.0g, pH buffer 0.5g, emulsifier 1.5g, deionized water 50g, stir evenly to make acrylate pre-emulsion; 0.4g potassium persulfate in 8.0g deionized water Dissolve and prepare initiator solution; Add 100g of the above-mentioned polymer silicone emulsion, 30.0g of butyl acrylate, 20.0g of isooctyl acrylate, 10.0g of methyl methacrylate, 5.0g of acrylonitrile, di 1.5 g of ethylene glycol methacrylate was heated up to 30°C. Swell under stirring for 12 hours; heat up to 50°C, add 6g of the above-mentioned initiator solution, and heat up to 78°C, after the emulsion in the polymerization reactor has blue light, then continuously add the remaining pre-emulsion to the polymerization reactor for 2 hours. After the a...

Embodiment 2

[0076] Heat up 62.0g of cooling silicone oil emulsion H-424, 30g of deionized water to 40°C, and stir evenly for 2 hours to obtain the first component; 40.0g of butyl acrylate, 10.0g of ethyl acrylate, and 10.0g of methyl methacrylate g, acrylonitrile 3.0g, styrene 2.0g, pH buffer 0.5g, emulsifier 1.5g, deionized water 50g, stir evenly to make acrylate pre-emulsion; dissolve 0.35g potassium persulfate in 7.0g deionized water , to prepare an initiator solution; add 90 g of the above-mentioned polymer silicone emulsion, 40.0 g of butyl acrylate, 10.0 g of ethyl acrylate, 10.0 g of methyl methacrylate, 3.0 g of acrylonitrile, and 2.0 g of styrene in the polymerization reactor. g, 1.5 g of ethylene glycol dimethacrylate, heated up to 30°C. Swell under stirring for 12 hours; raise the temperature to 50°C, add 4.5g of the above-mentioned initiator solution, and raise the temperature to 78°C, after the emulsion in the polymerization reactor has blue light, then continuously drop the ...

Embodiment 3

[0080] Heat up 50.0g of cooling silicone oil emulsion SOFTEX S-009, 1.5g of emulsifier, and 50.0g of deionized water to 40°C, and stir evenly for 2 hours to obtain the first component; 40.0g of butyl acrylate, 5.0 g of isooctyl acrylate g, methyl methacrylate 5.0g, styrene 3.0g, methylenebisacrylamide 1.5g, pH buffer 0.5g, emulsifier 1.6g, deionized water 50g, stir evenly to make acrylate pre-emulsion; 0.5g potassium persulfate is dissolved in 9.0g deionized water, and is mixed with initiator solution; Add above-mentioned polymer silicone emulsion 100g, butyl acrylate 40.0g, isooctyl acrylate 5.0g, methacrylic acid in polymerization reactor Methyl ester 5.0g, styrene 3.0g, methylenebisacrylamide 1.0g, heat up to 30°C, swell for 12h under stirring; heat up to 50°C, add 6g of the above-mentioned initiator solution, heat up to 80°C, wait for polymerization After the blue light appeared in the emulsion in the kettle, add the remaining pre-emulsion to the polymerization reaction ke...

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Abstract

The invention discloses a printing adhesive and a preparation method thereof, printing paste and clothing. The printing adhesive is prepared from the following components in parts by weight: 40-70 parts of a cool silicone emulsion, 0.6-1.0 part of an emulsifier, 36-59 parts of deionized water, 80-100 parts of soft monomer, 10-30 parts of a hard monomer, 0.6-3.0 parts of an emulsifier, 0.2-0.6 part of a pH buffer agent, 50-60 parts of deionized water, 0.2-0.6 part of an initiator and 1-4 parts of a cross-linking monomer. The printing adhesive has the advantages of low viscosity and good heat dispersion and has a relatively high polymerization reaction rate, and the obtained polymer is high in molecular weight.

Description

technical field [0001] The invention relates to the field of light industry textiles, in particular to a printing adhesive and a preparation method thereof. Background technique [0002] Pigment printing is a special printing method that adheres non-affinity and reactive pigments to the surface of fibers by means of adhesives to form desired patterns. Pigment printing has the advantages of simple process, energy saving and less environmental pollution. At present, global pigment printing fabrics account for more than 70% of the total output of printed cloth. [0003] In recent years, my country's pigment printing has also made great progress, but the product structure is not yet reasonable. Most of the middle and low-end products have meager profits. The quality and grade of pigment printing products depend largely on the performance of pigment printing adhesives. [0004] The water-based polyacrylate PA adhesives used in the prior art are a large category of printing adhe...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06P1/52C08F220/18C08F220/14C08F220/44C08F212/08C08F222/14C08F222/38C08F2/26C08F2/30
CPCD06P1/525D06P1/5292C08F2/26C08F2/30C08F220/18C08F220/1804C08F220/1808C08F220/14C08F220/44C08F222/102C08F212/08C08F222/385C08F220/1802
Inventor 钟欣汪荣华赖世贤
Owner XIAMEN ANTA SPORTS GOODS CO LTD
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