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Preparation method of equal-thickness ultrafine grain TC4 titanium alloy plate

A technology for titanium alloy plates and titanium alloys, applied in the field of metallurgy, can solve the problems of incompleteness, deformation, cracking and welding, and difficulty in realizing fine-grained structure, so as to eliminate interfacial oxidation, improve interfacial bonding strength, and eliminate oxide scale and oil pollution. Effect

Inactive Publication Date: 2017-08-11
NORTHEASTERN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0006] The purpose of the present invention is to provide a method for preparing ultra-fine-grained TC4 titanium alloy plates with equal thickness, which can overcome the problem that the fine-grained structure is difficult to achieve due to insufficient deformation, and maintain the original thickness size. Due to the shortcomings of deformation cracking and incomplete welding, the prepared TC4 titanium alloy plate has high strength and high interface bonding strength

Method used

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  • Preparation method of equal-thickness ultrafine grain TC4 titanium alloy plate
  • Preparation method of equal-thickness ultrafine grain TC4 titanium alloy plate
  • Preparation method of equal-thickness ultrafine grain TC4 titanium alloy plate

Examples

Experimental program
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Effect test

Embodiment 1

[0032] Provide a kind of preparation method of ultra-fine grain TC4 titanium alloy sheet material in the present embodiment, this preparation method comprises the following steps:

[0033] S1, select 16 TC4 titanium alloy slabs with the same size (that is, the length, width and thickness of each TC4 titanium alloy slab are the same) and rolled and annealed, the thickness of the TC4 titanium alloy slab is 1mm, and the grain The size lies in the range of 6-10 μm.

[0034] S2. Divide all current TC4 titanium alloy slabs into 4 groups on average, and the number of TC4 titanium alloy slabs in each group is 4 pieces.

[0035] S3. Grinding and cleaning the interface of all the current TC4 titanium alloy slabs ("interface" is the surface of the TC4 titanium alloy slab to be bonded with other slabs in the subsequent steps) with alcohol or acetone. After the grinding treatment and cleaning are completed, dry, and then perform the following step S4 for each group of TC4 titanium alloy s...

Embodiment 2

[0043] In this embodiment, the preparation method of the ultra-fine-grained TC4 titanium alloy plate with equal thickness of the present invention is repeated by changing some parameters of the first embodiment above. details as follows:

[0044] S1. Select 27 TC4 titanium alloy slabs of the same size after rolling and annealing. The thickness of the TC4 titanium alloy slabs is 2 mm, and the grain size is in the range of 6-10 μm.

[0045] S2. Divide all current TC4 titanium alloy slabs into 9 groups on average, and the number of TC4 titanium alloy slabs in each group is 3.

[0046] S3. Grinding the interfaces of all current TC4 titanium alloy slabs (27 in total) and cleaning the surface with alcohol or acetone. After the grinding and cleaning are completed, dry, and then perform the following step S4 for each group of TC4 titanium alloy slabs, that is, perform step S4 once for 9 groups of TC4 titanium alloy slabs;

[0047] S4, a group of TC4 titanium alloy slabs are aligned ...

Embodiment 3

[0060] In this embodiment, the preparation method of the ultra-fine-grained TC4 titanium alloy plate with equal thickness of the present invention is repeated by changing some parameters of the first embodiment above. details as follows:

[0061] S1. Select 32 TC4 titanium alloy slabs with the same size and after rolling and annealing. The thickness of the TC4 titanium alloy slabs is 4 mm, and the grain size is in the range of 6-10 μm.

[0062] S2. Divide all current TC4 titanium alloy slabs into 16 groups on average, and the number of TC4 titanium alloy slabs in each group is 2.

[0063] S3. Grinding the interface of all current TC4 titanium alloy slabs and cleaning the surface with alcohol or acetone. After the grinding treatment and cleaning are completed, dry, and then perform the following step S4 for each group of TC4 titanium alloy slabs, that is, perform step S4 once for 16 groups of TC4 titanium alloy slabs;

[0064] S4. Align and stack a group of TC4 titanium alloy...

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Abstract

The invention relates to the technical field of metallurgy, in particular to a preparation method of an equal-thickness ultrafine grain TC4 titanium alloy plate. The preparation method comprises the steps that S1, plate blanks obtained after rolling and annealing are taken; S2, the plate blanks are grouped; S3, interfaces of the plate blanks are subjected to roughening treatment and cleaning, and then the following operation of S4 is executed on each group; S4, the plate blanks in each group are stacked into a plate layer, one side edge of each plate layer is welded, the other side edges of each plate layer are coated with anti-oxidation coatings, or all edges of the plate layers are subjected to vacuum seal welding, the hot rolling process is adopted for ply rolling and welding, final hot rolling is carried out till the thickness of the plate layers is equal to the original thickness of the plate blanks, and then air cooling is carried out; S5, if the plate layers need to be grouped again, the plate layers serve as new plate blanks to return to the step S2, and otherwise all the plate layers form a plate blank group to return to the step S3 till all the plate blanks are subjected to ply rolling into the plate; S6, the plate is subjected to heat treatment and then cooled. According to the method, the defects of the insufficient hot rolling deformation and deformation cracking and incomplete welding in the ply rolling process can be overcome, and the equal-thickness ultrafine grain plate can be prepared.

Description

technical field [0001] The invention relates to the technical field of metallurgy, in particular to a method for preparing an ultrafine-grained TC4 titanium alloy plate with equal thickness. Background technique [0002] TC4 (Ti-6Al-4V) titanium alloy has comprehensive properties such as low density, excellent high-temperature strength, biocompatibility, and corrosion resistance, and is widely used in many fields such as aerospace, automobile, and medical treatment. The preparation of ultra-fine-grained titanium alloy can significantly improve the mechanical properties, biocompatibility and superplastic forming ability. Become the key to expand the application field of titanium alloy. Wherein, the grain size of the ultrafine crystal is in the range of 0.1-1 μm. [0003] For the grain refinement of titanium alloys, the method of large plastic deformation is usually adopted at home and abroad to increase the processing deformation of the alloy in the two-phase region as much...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B21B1/38B21B3/00B23K37/00
CPCB21B1/38B21B3/00B21B2001/386B23K37/00
Inventor 刘国怀王昭东李勇李天瑞徐莽付天亮王丙兴
Owner NORTHEASTERN UNIV
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