Phosphorus-nitrogen-containing polymer-coated beta-FeOOH nanoparticles, and preparation method and application thereof
A nanoparticle and polymer technology, applied in the field of flame retardant rubber, can solve problems such as the inability to meet the requirements of practical applications, the decline of rubber mechanical properties, etc., and achieve the effect of good smoke suppression, overcoming poor compatibility, and improving thermal stability.
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Embodiment 1
[0029] (1) Add 17.1g FeCl to the single-necked bottle in turn 3 ·6H 2 0. 15 g of polyvinylpyrrolidone and 600 mL of water were reacted at 80° C. for 10 h. After centrifugation, the supernatant was discarded to leave a precipitate, and the resulting precipitate was washed repeatedly with water and ethanol to obtain nanometer β-FeOOH.
[0030] (2) Get 10g of nanometer β-FeOOH obtained in step (1) and disperse it in the first solvent, add 20g of 3,4-dihydroxybenzaldehyde, stir at room temperature for 6h, pour off the clear liquid after centrifugation and leave the precipitate, the resulting precipitate The substance is reacted and washed with the first solvent to obtain 3,4-dihydroxybenzaldehyde-modified β-FeOOH.
[0031] (3) Disperse 1 g of 3,4-dihydroxybenzaldehyde-modified β-FeOOH obtained in step (2) and 0.2 g of terephthalaldehyde in 600 mL of tetrahydrofuran, and then slowly add 720 mL of 0.01 g / mL dissolved in 2,4,6-tris(p-N'-octadecylureido-anilino)-1,3,5-triazine solut...
Embodiment 2
[0034] (1) The preparation of nanometer β-FeOOH is the same as in Example 1.
[0035] (2) The preparation of 3,4-dihydroxybenzaldehyde-modified β-FeOOH is the same as in Example 1.
[0036] (3) The preparation of β-FeOOH nanoparticles coated with phosphorus and nitrogen polymer is the same as that in Example 1.
[0037] (4) Take 0.5g of phosphorus-nitrogen-containing polymer-coated β-FeOOH nanoparticles and blend them with 100g of rubber, ultrasonically treat them for 0.5-3 hours, add 2g of DCP, mix them on an open mill for 5-10 minutes, and then mold and vulcanize them to obtain phosphorus-containing Nitrogen polymer coated β-FeOOH nanoparticles functionalized flame retardant rubber.
Embodiment 3
[0039] (1) The preparation of nanometer β-FeOOH is the same as in Example 1.
[0040] (2) The preparation of 3,4-dihydroxybenzaldehyde-modified β-FeOOH is the same as in Example 1.
[0041] (3) The preparation of β-FeOOH nanoparticles coated with phosphorus and nitrogen polymer is the same as that in Example 1.
[0042] (4) Take 0.25g of phosphorus-nitrogen-containing polymer-coated β-FeOOH nanoparticles and blend them with 100g of rubber, ultrasonically treat them for 0.5-3 hours, add 2g of DCP, mix them on an open mill for 5-10 minutes, and then mold and vulcanize them to obtain phosphorus-containing Nitrogen polymer coated β-FeOOH nanoparticles functionalized flame retardant rubber.
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