Preparation method of high-color-rendering white phosphor for 3D (three-dimensional) printing

A 3D printing and high color rendering technology, applied in chemical instruments and methods, luminescent materials, climate sustainability, etc., can solve problems such as short device life and difficulty in forming LED light-emitting layers, achieving high precision and accurate and detailed data , the effect of advanced technology

Active Publication Date: 2017-09-05
TAIYUAN UNIV OF TECH
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  • Abstract
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  • Application Information

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Problems solved by technology

[0003] As a kind of composite light, white light can effectively excite red, green, and blue primary color phosphors to emit their own characteristic monochromatic light through high-energy short-wavelength ultraviolet light, and finally compound to obtain white light; The technology of obtaining white light has high color rendering, and the current technology of preparing tri-primary white phosphors with high color rendering index

Method used

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  • Preparation method of high-color-rendering white phosphor for 3D (three-dimensional) printing
  • Preparation method of high-color-rendering white phosphor for 3D (three-dimensional) printing
  • Preparation method of high-color-rendering white phosphor for 3D (three-dimensional) printing

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Embodiment Construction

[0076] The present invention will be further described below in conjunction with accompanying drawing:

[0077] figure 1 As shown, the state diagram for the preparation of the polymer, the position of each part must be correct, the proportion should be proportioned, and the operations should be performed in sequence.

[0078] Quantities of chemicals used in preparation are determined in pre-set ranges in grams, milliliters, centimeters 3 is the unit of measurement.

[0079] The preparation of the polymer is carried out in a three-necked flask, which is completed in a water bath, heating, magnetic stirring, nitrogen protection, and water circulation condensation;

[0080] The electric heater 1 is vertical, and the upper part of the electric heater 1 is a water bath 2, and the upper part of the water bath 2 is a three-necked flask 3, which is fixed by a fixing seat 21. The water bath 2 is a water bath 4, and the water bath 4 needs Submerge 4 / 5 of the volume of the three-necke...

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Abstract

The invention relates to a preparation method of high-color-rendering white phosphor for 3D (three-dimensional) printing, and aims to solve the problems of high color temperature, low color rendering index and poor film forming performance of the white phosphor. The method includes the steps: taking 2-thenoyltrifluoroacetone-phenanthroline-europium, 4-benzoyl benzoic acid-terbium, benzothiazole-zinc and polystyrene-methacrylic acid glycidyl ester as raw materials; performing physical blending, heating and melting, drying, grinding and screening on the raw materials to prepare the high-color-rendering white phosphor, the particle diameter of the white phosphor is smaller than or equal to 1 micrometer, the prepared white phosphor materials are high in accuracy and good in purity, the purity of the white phosphor materials reach 99.8%, color coordinates X=0.332, Y=0.337, white light is emitted, the preparation method is advanced in process, data are detailed and accurate, and the advanced preparation method is used for the high-color-rendering white phosphor for 3D printing.

Description

technical field [0001] The invention relates to a method for preparing a high-color-rendering white phosphor powder for 3D printing, which belongs to the technical field of preparation and application of luminescent materials. Background technique [0002] White light-emitting diodes (LEDs) are known as the fourth-generation green lighting sources because of their small size, low energy consumption, and long life, and have been widely used in industrial and civilian products. [0003] As a kind of composite light, white light can effectively excite red, green, and blue primary color phosphors to emit their own characteristic monochromatic light through high-energy short-wavelength ultraviolet light, and finally compound to obtain white light; The technology of obtaining white light has high color rendering, and the current technology of preparing tri-primary white phosphors with high color rendering index needs to be broken through; in addition, the production of LED light-e...

Claims

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Application Information

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IPC IPC(8): C09K11/06C08F8/42C08F220/32C08F212/08B33Y70/00
CPCB33Y70/00C08F8/42C08F220/32C08F220/325C09K11/06C09K2211/1425C09K2211/145C09K2211/1458C09K2211/1483C09K2211/182C09K2211/188C08F212/08Y02B20/00
Inventor 张爱琴贾虎生王滨李栋信申倩倩刘旭光许并社
Owner TAIYUAN UNIV OF TECH
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