Method for preparing chemical sand solidification agent
A sand-fixing agent and chemical technology, which is applied in the field of preparation of chemical sand-fixing agents, can solve the problems of poor water retention and sand-fixing ability, and achieve the effect of strong water retention and enhanced sand-fixing effect
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example 1
[0024] Weigh 40g itaconic acid, 15g acrylic acid and 200mL absolute ethanol into the flask, place the flask in a water bath, control the temperature of the water bath to 60°C, then add 0.1g ammonium persulfate to the flask, keep stirring for 2h, After the reaction is completed, the material in the flask is placed in a rotary evaporator, and the concentrated solution is concentrated by rotary evaporation for 30min to obtain a concentrated solution containing itaconic acid acrylic acid copolymer, and the concentrated solution containing itaconic acid acrylic acid copolymer is placed in the flask, Then 200 mL of thionyl chloride was added to the flask, and the flask was moved into a constant temperature digital display magnetic stirrer, and the reaction was stirred for 1 h at a temperature of 80 °C and a rotation speed of 300 r / min. After the reaction was completed, the product was placed in a rotating In an evaporator, rotary evaporation is concentrated to dryness to obtain a dry...
example 2
[0026]Weigh 50g of itaconic acid, 20g of acrylic acid and 300mL of absolute ethanol into the flask, place the flask in a water bath, control the temperature of the water bath to be 70°C, then add 0.3g of dicumyl peroxide to the flask, keep stirring Reaction for 3h, after the reaction is completed, the material in the flask is placed in a rotary evaporator, and concentrated by rotary evaporation for 40min to obtain a concentrated solution containing itaconic acid acrylic acid copolymer, and the concentrated solution containing itaconic acid acrylic acid copolymer is placed in In the flask, add 300 mL of thionyl chloride to the flask, move the flask into a constant temperature digital display magnetic stirrer, and stir the reaction for 2 hours at a temperature of 90 ° C and a rotation speed of 400 r / min. Placed in a rotary evaporator, and concentrated to dryness by rotary evaporation to obtain a dried product containing itaconic chloride acryloyl chloride copolymer, and 300 mL of...
example 3
[0028] Weigh 45g of itaconic acid, 18g of acrylic acid and 250mL of absolute ethanol into the flask, place the flask in a water bath, control the temperature of the water bath to be 65°C, then add 0.2g of benzoyl peroxide to the flask, keep stirring for the reaction 2.5h, after the reaction is over, place the material in the flask in a rotary evaporator, and rotate and concentrate for 35min to obtain a concentrated solution containing itaconic acid-acrylic acid copolymer, and the concentrated solution containing itaconic acid-acrylic acid copolymer is placed in In the flask, add 250 mL of thionyl chloride to the flask, move the flask into a constant temperature digital display magnetic stirrer, and stir the reaction for 1.5 h at a temperature of 85 °C and a rotation speed of 350 r / min. The product was placed in a rotary evaporator, and concentrated to dryness by rotary evaporation to obtain a dried product containing itaconic acid chloride acryloyl chloride copolymer, and 250 m...
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