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Method for preparing loquat-flower tobacco flavor through combined high hydrostatic pressure and enzymatic hydrolysis, and application of loquat-flower tobacco flavor

A technology for tobacco flavors and loquat flowers, which is applied in the field of tobacco flavors, can solve the problems of few high static pressure technologies and no relevant reports, and achieve the effects of improving product aroma quality, improving extraction efficiency, and avoiding loss and deterioration.

Active Publication Date: 2017-09-15
CHINA TOBACCO JIANGXI IND CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In view of the effect of high static pressure technology on the physical properties of materials, some scholars have used this technology to conduct research on agricultural products and food, such as "A Method for Preparing Resistant Starch Using High Static Pressure Treatment of B-type Starch", Patent No. 201610067856.X; "A Method for Preparing Hypoallergenic Ginkgo Protein Powder by High Static Pressure Combined with Enzymatic Hydrolysis", Patent No. 201610161399.0; "A Non-thermal Processing Method for Clear Strawberry Juice", Patent No. 201010217124.7; But so far, The application of high static pressure technology in the development of flavors and fragrances for tobacco is less, and it is only found in the field of Maillard reaction synthesis of flavors, such as Patent No. 201310270886.7 "A method for preparing Maillard reaction type tobacco flavors by using high static pressure" , but in the field of organic extraction of tobacco flavors, especially in the extraction of floral heat-sensitive tobacco flavors, there are almost no related reports

Method used

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  • Method for preparing loquat-flower tobacco flavor through combined high hydrostatic pressure and enzymatic hydrolysis, and application of loquat-flower tobacco flavor

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Take 100g of fresh loquat flowers, wash them, chop them up, add 400g of water, 0.2g of compound enzymes (including 0.1g of β-glucosidase, 0.05g of cellulase, and 0.05g of glucoamylase) to it, and shake in a water bath at 50°C. Enzymolysis in bed for 4h; after enzymolysis, add 400g of 1,2-propanediol, shake and shake well, place in 65℃ water bath for 4h; put the loquat flower substrate and extract together into a sealed double-layer poly Put it in the ethylene high-temperature cooking bag, after vacuuming, put it in the high static pressure equipment (with pure water as the pressure transmission medium) at 50 ℃ for high static pressure treatment for 30min, the treatment pressure is 300MPa; finally, the high static pressure treatment The final loquat flower extract is suction-filtered to obtain the filtrate, and potassium sorbate with a filtrate quality of 0.2% is added to the filtrate, and packaged to obtain the loquat flower tobacco flavor 1;

Embodiment 2

[0027] Take 100g of fresh loquat flowers, wash them, chop them, add 400g of water, 0.2g of complex enzymes (including 0.05g of β-glucosidase, 0.1g of cellulase, and 0.05g of glucoamylase) to it, and shake in a water bath at 50°C. Enzymolysis in bed for 4h; after enzymolysis, add 400g of 1,2-propanediol, shake and shake well, place in 65℃ water bath for 4h; put the loquat flower substrate and extract together into a sealed double-layer poly Put it in the ethylene high-temperature cooking bag, after vacuuming, put it in the high static pressure equipment (with pure water as the pressure transmission medium) at 50 ℃ for high static pressure treatment for 30min, the treatment pressure is 300MPa; finally, the high static pressure treatment The final loquat flower extract is suction-filtered to obtain the filtrate, and potassium sorbate with a filtrate quality of 0.2% is added to the filtrate, and the package is obtained to obtain the loquat flower flavor for tobacco 2;

Embodiment 3

[0029] Take 100g of fresh loquat flowers, wash them, chop them up, add 400g of water, 0.2g of compound enzymes (including 0.1g of β-glucosidase, 0.05g of cellulase, and 0.05g of glucoamylase) to it, and shake in a water bath at 50°C. Enzymolysis in the bed for 2 hours; after the completion of the enzymolysis, add 300g of 1,2-propanediol, oscillate, place in a water bath at 60°C for 6 hours; put the loquat flower substrate and extract together into a sealed double-layer polythene Put it in the ethylene high-temperature cooking bag, after vacuuming, put it in the high static pressure equipment (with pure water as the pressure transmission medium) at 50 ℃ for high static pressure treatment for 30min, the treatment pressure is 300MPa; finally, the high static pressure treatment The final loquat flower extract is suction-filtered to obtain the filtrate, and potassium sorbate with a filtrate quality of 0.2% is added to the filtrate, and the package is obtained to obtain the loquat fl...

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Abstract

The invention especially relates to a method for preparing a loquat-flower tobacco flavor through combined high hydrostatic pressure and enzymatic hydrolysis, and application of the loquat-flower tobacco flavor, belonging to the technical field of tobacco flavors. The preparation method for the loquat-flower tobacco flavor comprises the following steps: pretreatment; enzymatic hydrolysis; composite extraction with propylene glycol and water; high-hydrostatic-pressure-process secondary extraction; filtering and packaging; etc. According to the invention, a heat-sensitive substrate (fresh loquat flowers) is used as a raw material, treatment with a compound enzyme is carried out at first; then propylene glycol is employed to maximally acquire fat-soluble aroma components in the loquat flowers; and high-hydrostatic-pressure-process secondary extraction is finally carried out to effectively improve the aroma quality of the obtained tobacco flavor and to deactivate enzymes, so the step of high-temperature enzyme deactivation is avoided, and loss and deterioration of aroma components of the heat-sensitive flowers are prevented. The loquat-flower tobacco flavor prepared in the invention is applied to tobacco flavoring and can substantially enhance the richness of tobacco flavors and sweetness of cigarettes.

Description

technical field [0001] The invention belongs to the technical field of tobacco spices, and in particular relates to a method and application for preparing loquat flower tobacco spices through high static pressure coordinated enzymatic hydrolysis. Background technique [0002] Loquat flower is the flower of Rosaceae plant Loquat, which has a fragrant and slightly sweet smell and contains a variety of vitamins. According to the "Compendium of Materia Medica", loquat flower has the effects of "quenching thirst and lowering qi, benefiting the lungs, stopping vomiting, removing scorched heat, moistening the five internal organs" and "curing head wind and clearing the nose". In view of loquat flower's functions of moisturizing the throat, moistening the lungs, resolving phlegm and relieving cough, clearing fire and relieving heat, it is mostly used in tea making and Chinese medicine processing, but it is rarely used in the preparation of cigarette flavors and fragrances. [0003]...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/00A24B3/12
CPCA24B3/12C11B9/00
Inventor 徐达李赓苏加坤罗海涛胡巍耀何力郭磊罗娟敏蔡继宝罗凌超
Owner CHINA TOBACCO JIANGXI IND CO LTD