Preparation method of acidulant special for feeds
A technology of acidifier and feed, which is applied in the field of preparation of special acidifier for feed, which can solve the problems of unreachable and difficult to decompose, and achieve the effects of fast decomposition, low cost and long shelf life
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Embodiment 1
[0016] A kind of preparation method of special acidifier for feed, its preparation method is as follows:
[0017] A. Mix lactic acid and citric acid according to a certain ratio of 1:1, stir evenly, slowly add an appropriate amount of fumaric acid, the stirring speed is 600r / min, and the temperature is set at 45°C;
[0018] B. The polycondensation reaction of lactic acid through esterification reaction under the action of a catalyst to generate polylactic acid, the temperature is controlled at 20-30°C, the pressure is 1000-1200pa, and the time is 1-2h;
[0019] C, adopt acetic acid to regulate the pH value of the mixture in step A, keep on 5.0;
[0020] D, adding phosphoric acid to the product in step C, using silicon dioxide as a carrier for adsorption, and using polylactic acid in step B as an adhesive to bond to form a white powdery product;
[0021] E. Compress and dry the product in step D to produce a granular product, set the temperature at 60° C., and perform ultravio...
Embodiment 2
[0025] A kind of preparation method of special acidifier for feed, its preparation method is as follows:
[0026] A. Mix lactic acid and citric acid according to a certain ratio of 1:1, stir evenly, slowly add an appropriate amount of fumaric acid, the stirring speed is 550r / min, and the temperature is set at 45°C;
[0027] B. Polylactic acid is generated by polycondensation of lactic acid through esterification reaction under the action of a catalyst, the temperature is controlled at 24°C, the pressure is 1100pa, and the time is 1.2h;
[0028] C, adopt acetic acid to regulate the pH value of the mixture in step A, keep on 4.5;
[0029] D, adding phosphoric acid to the product in step C, using silicon dioxide as a carrier for adsorption, and using polylactic acid in step B as an adhesive to bond to form a white powdery product;
[0030] E. Compress and dry the product in step D to produce a granular product, set the temperature at 75° C., and perform ultraviolet disinfection ...
Embodiment 3
[0034] A kind of preparation method of special acidifier for feed, its preparation method is as follows:
[0035] A. Mix lactic acid and citric acid according to a certain ratio of 1:1, stir evenly, slowly add an appropriate amount of fumaric acid, the stirring speed is 800r / min, and the temperature is set to 30°C;
[0036] B. Polylactic acid is generated by polycondensation of lactic acid through esterification under the action of a catalyst, the temperature is controlled at 30°C, the pressure is 1200pa, and the time is 1h;
[0037] C, adopt acetic acid to regulate the pH value of the mixture in step A, keep on 6.0;
[0038] D, adding phosphoric acid to the product in step C, using silicon dioxide as a carrier for adsorption, and using polylactic acid in step B as an adhesive to bond to form a white powdery product;
[0039] E. Compress and dry the product in step D to produce a granular product, set the temperature at 50° C., and perform ultraviolet disinfection for 5 minut...
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