Three-dimensional structured micropore material and preparation method therefor

A technology of microporous materials and three-dimensional structures, applied in electrolytic coatings, metal processing equipment, magnetic layers, etc., can solve the problems that cannot further reduce the thickness of equipment, increase the overall manufacturing cost of equipment, occupy equipment assembly space, etc., and achieve space heat conduction and Good impact resistance, solve the comprehensive problem of heat conduction and electromagnetic shielding, good consistency

Active Publication Date: 2017-11-21
山东中科绿碳科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The existing solution to equipment heating and electromagnetic shielding is to use electromagnetic shielding components and heat conduction and heat dissipation components in combination, which not only increases the overall manufacturing cost of the equipment, but also uses multiple compo

Method used

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  • Three-dimensional structured micropore material and preparation method therefor
  • Three-dimensional structured micropore material and preparation method therefor
  • Three-dimensional structured micropore material and preparation method therefor

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] A preparation method of a three-dimensional structure microporous material is carried out according to the following steps:

[0028] Ⅰ Mix the spherical graphite powder with a particle size of 1nm and the spherical nickel powder with a particle size of 0.1nm at a mass ratio of 5:1 and then use a ball mill for ball milling. The ball milling speed is 5000 rpm and the ball milling time is 5 hours. The surface of the graphite powder is coated with a layer of nickel powder with a thickness of 0.1 μm to obtain a magnetic microsphere graphite powder; the prepared magnetic microsphere graphite powder is dissolved in ethylene glycol with a concentration of 1% to make a magnetic microsphere Spherical graphite powder solution;

[0029] ⅡThrough the conventional chemical plating method, a nickel layer with a thickness of 0.1 μm is plated on the surface of carbon nanotubes with a length of 1 nm and a diameter of 0.5 nm to prepare magnetically conductive carbon nanotubes; the prepare...

Embodiment 2

[0039] A method for preparing a three-dimensional microporous material, the steps of which are similar to those of the method for preparing a three-dimensional microporous material in Example 1, except that:

[0040] 1. In step I, the particle size of the spherical graphite powder is 70nm, the particle size of the spherical nickel powder is 30nm, the mass ratio of the spherical graphite powder to the spherical nickel powder is 7:3, the ball milling speed is 7000 rpm, and the ball milling time is 7 hours, the surface of the graphite powder is coated with a layer of nickel powder with a thickness of 0.5 μm;

[0041] 2. In step II, the carbon nanotubes have a length of 2.5 nm and a diameter of 2.5 nm, and the surface of the carbon nanotubes is coated with a nickel layer with a thickness of 0.5 μm;

[0042] 3. In step Ⅲ, the polymer microporous matrix material adopts a polyurethane film with a thickness of 2.5 μm, a pore diameter of 5 μm, a porosity of 70%, and a pore spacing of 2...

Embodiment 3

[0051] A method for preparing a three-dimensional microporous material, the steps of which are similar to those of the method for preparing a three-dimensional microporous material in Example 1, except that:

[0052] 1. In step I, the particle size of the spherical graphite powder is 0.1 μm, the particle size of the spherical nickel powder is 50 nm, the mass ratio of the spherical graphite powder to the spherical nickel powder is 9:5, the ball milling speed is 9000 rpm, and the ball milling time is After 10 hours, the surface of the graphite powder is coated with a layer of nickel powder with a thickness of 1.0 μm; the organic solvent is isopropanol with a concentration of 10%;

[0053] 2. In step II, the carbon nanotubes have a length of 5 nm and a diameter of 5 nm, and the surface of the carbon nanotubes is coated with an iron layer with a thickness of 1 μm; the organic solvent is isopropanol with a concentration of 10%;

[0054] 3. In step III, the macromolecular microporou...

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Abstract

The invention provides a three-dimensional structured micropore material. The three-dimensional structured micropore material adopts a three-dimensional net-shaped structure entirely; magnetic conductive microsphere powder is arranged in X, Y and Z directions in a magnetic control mode; the surface of the magnetic conductive microsphere powder is coated and loaded with magnetic conductive nanotubes; the gaps of the magnetic conductive microsphere powder are filled with magnetic conductive nanotubes; the overall surface is electrically deposited with a metal layer; and the micropores are 1-100nm in pore diameters and 0.1-5[mu]m in overall thickness. Meanwhile, the invention also provides a preparation method for the three-dimensional structured micropore material. The preparation method is simple in process and low in manufacturing cost; and the prepared material has creative structure, relatively uniform and ordered crystal structure arrangement, relative high material consistency, high space heat conduction and impact resistance of the material and the like.

Description

technical field [0001] The invention relates to a three-dimensional structure microporous material and a preparation method thereof, which are applied in the fields of electromagnetic shielding, heat transfer and heat dissipation, light weight and the like. Background technique [0002] Microporous materials, including zeolites and silicoaluminophosphates, are widely used in the petroleum industry as absorbents, catalysts, and catalyst supports. With the development of new material technology, all kinds of two-dimensional and three-dimensional space materials, as well as matrix arrangement materials and preparation technologies emerge in an endless stream, and have also achieved great development in various fields. In recent years, the research on the alignment technology of metal particles has become a research hotspot of new functional materials, but the materials prepared by the alignment technology of metal particles with three-dimensional structure have not been publish...

Claims

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Application Information

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IPC IPC(8): H01F10/12H01F10/14B22F1/02C25D5/56C25D15/00
CPCC25D5/006H01F10/12H01F10/14C25D5/56C25D15/00B22F1/17
Inventor 陈红辉
Owner 山东中科绿碳科技有限公司
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