Method for extracting effective components in dropped fruit of tangerines and tangerine peels
A technology of active ingredients and extraction method, applied in the field of extraction of active ingredients in plants, can solve the problems of single extraction and insufficient utilization of fallen citrus fruits, and achieve the effects of promoting further development, improving economic utilization value, and improving comprehensive utilization rate.
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specific Embodiment 1
[0022] A method for extracting active ingredients in citrus fruit drop and tangerine peel described in the present embodiment specifically comprises the following steps:
[0023] 1) Clean the fallen citrus fruits and orange peel, dry them at high temperature and crush them, and pass through a 60-mesh sieve to obtain the crushed raw materials. Mix the crushed raw materials and petroleum ether at a weight (kg) / volume ratio (L) of 1:25, 75 Reflux extraction at ℃ for 2 hours, filter once with a 0.2um ceramic membrane to obtain the filtrate, then concentrate under reduced pressure to remove petroleum ether, and then dry to obtain degreasing and pulverized raw materials;
[0024] 2) Extract the degreased pulverized raw material obtained in 1) with 75% ethanol at a weight / volume ratio of 1:3, extraction time is 2 hours, and countercurrently extract 3 times, use ultrasonic assisted extraction for each extraction, and filter with ceramic membrane after each extraction The filtrate was ...
specific Embodiment 2
[0032] A method for extracting active ingredients in citrus fruit drop and tangerine peel described in the present embodiment specifically comprises the following steps:
[0033] 1) Clean the fallen citrus fruits and orange peel, dry them at high temperature and crush them, and pass through a 60-mesh sieve to obtain the crushed raw materials. Mix the crushed raw materials and petroleum ether at a weight (kg) / volume ratio (L) of 1:30, 70 Reflux extraction at ℃ for 2.5 hours, filter once with a 0.2um ceramic membrane to obtain the filtrate, then concentrate under reduced pressure to remove petroleum ether, and then dry to obtain degreasing pulverized raw materials;
[0034] 2) Extract the degreased pulverized raw material obtained in 1) with 75% ethanol at a weight / volume ratio of 1:4, extracting time 2.5 hours countercurrently for 3 times, use ultrasonic assisted extraction for each extraction, and use ceramic membrane after each extraction Filtrate to obtain the filtrate, comb...
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