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A Cementing-Formation Solidification Integrated Fluid Applied to Deep Water Weakly Consolidated Formation

A weakly cemented, formation technology, applied in the directions of drilling compositions, chemical instruments and methods, etc., can solve the problem that the target interval cannot be fully solidified, and it is difficult to ensure the contact time between the solidified slurry and the formation, and the grouting pipe It is difficult to solve the problems of placement and recycling, and achieves high environmental protection and economic benefits, improved curing strength, and good dispersibility.

Active Publication Date: 2020-11-27
CHINA UNIV OF PETROLEUM (EAST CHINA)
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, solidifying the formation while solidifying the annulus will make it difficult to implement the injection process of the solidified grout. The main system is in the following three points: 1. If the conventional grouting reinforcement technology is used to pump the solidified grout into the grouting pipe, the placement and recovery of the grouting pipe Difficult to solve
2. If the solidified slurry is used to wash the formation in the annular space by means of pressurized circulation, it is difficult to ensure the contact time between the solidified slurry and the formation, and the good effect of fully solidifying the target layer cannot be achieved.
3. If the solidified slurry is added to the cement slurry, due to the difference in properties between the solidified slurry and the cement slurry, the hydration of the cement slurry will be greatly affected, thereby affecting the cementing quality of the weakly cemented formation
However, the existing technology cannot achieve a good curing effect on the formation on the basis of meeting the requirements of cementing construction.

Method used

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  • A Cementing-Formation Solidification Integrated Fluid Applied to Deep Water Weakly Consolidated Formation
  • A Cementing-Formation Solidification Integrated Fluid Applied to Deep Water Weakly Consolidated Formation
  • A Cementing-Formation Solidification Integrated Fluid Applied to Deep Water Weakly Consolidated Formation

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] The mass ratio of each component of the cementing-solidification integrated fluid is:

[0030] 400g of ultrafine slag (1250 mesh), 320g of water, 24g of sodium hydroxide, 7.6g of epoxy resin, 12.4g of curing agent, 40g of hollow glass microspheres, 2.4g of silane coupling agent, denoted as GR1.

[0031] Stir and mix evenly to prepare the cementing-curing integrated fluid slurry specimen, measure the setting time at 15°C, and the compressive strength at 7°C and 24h curing at 15°C.

[0032] Weigh respectively 15% and 20% cementing-curing integrated fluid to prepare soft soil solidified samples, weigh 700g of prepared soil samples, mix and stir evenly to obtain solidified soil samples, measure at 7°C, 15°C Under curing for 7 days unconfined compressive strength.

Embodiment 2

[0034] The content of each component of the cementing-solidification integrated fluid is changed, and the others are the same as in Example 1. The mass ratio of the components of the cementing-solidification integrated fluid is: 400g of ultrafine slag (1250 mesh), 320g of water, and 24g of sodium hydroxide , epoxy resin 15.2g, curing agent 24.8g, 40g hollow glass microspheres, 2.4g silane coupling agent, denoted as GR2.

Embodiment 3

[0036] The content of each component of the cementing-solidification integrated fluid is changed, and the others are the same as in Example 1. The mass ratio of the components of the cementing-solidification integrated fluid is: 400g of ultrafine slag (1250 mesh), 360g of water, and 24g of sodium hydroxide , epoxy resin 7.6g, curing agent 12.4g, 40g hollow glass microspheres, 2.4g silane coupling agent, denoted as GR3.

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Abstract

The invention provides well cementation and formation solidification integrated liquid applied to a deepwater weakly consolidated formation. The well cementation and formation solidification integrated liquid applied to the deepwater weakly consolidated formation is characterized by comprising the following components in parts by weight: 100 parts of superfine granulated blast furnace slag, 5 to 40 parts of resin, 5 to 30 parts of hollow glass beads, 2 to 8 parts of sodium hydroxide or potassium hydroxide, 0.2 to 1 part of a silane coupling agent and 70 to 100 parts of water. The 24-hour compressive strength of the well cementation and formation solidification integrated liquid system is 3.5 MPa or higher; after the coupling agent, the hollow glass beads and the resin are added, the coagulation time of the integrated liquid system is greatly prolonged, the thickening time is 2 hours or longer and the flowability is 20 cm or larger. Meanwhile, the well cementation and formation solidification integrated liquid has high solidification effect on mud clay. Through addition of the hollow glass beads and increment of a water cement ratio, the flowability of slurry is enhanced and the coagulation time of the slurry is prolonged.

Description

technical field [0001] The invention belongs to the technical field of well cementing in deep-water weakly cemented formations, and in particular relates to a slag-resin-based solidifying liquid for well cementing in deep-water weakly cemented formations. Background technique [0002] In recent years, with the advancement of offshore drilling and production technology, my country's offshore oil industry has entered the deep-water era. In addition to deep-water offshore oil equipment, technology, and tools, deep-water cementing technology is to ensure the safe construction and long-term maintenance of deep-water offshore oil and gas drilling wells. One of the key technologies of life. Among them, whether deep-water weakly cemented formations can be effectively sealed for a long time is facing more challenges. For deep water cementing, the compaction conditions and temperature characteristics of deep formations are similar to those of conventional land or shallow sea formation...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K8/44
CPCC09K8/44
Inventor 步玉环杜嘉培柳华杰郭胜来田磊聚
Owner CHINA UNIV OF PETROLEUM (EAST CHINA)
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