A high-efficiency and energy-saving xylene separation process
A m-xylene and process technology, which is applied in the field of separation and purification of aromatic xylene, can solve problems such as unsatisfactory residence time, achieve the effects of saving reactor volume, long material residence time, and eliminating excessive reaction
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Embodiment 1
[0042] Raw material C8 aromatics plus xylene concentration 20wt%, HF and BF in the extractant 3 The concentration is 20wt%.
[0043] The feed ratio of extractant and C8 aromatics is 2:1 (volume ratio). The extractant and C8 aromatics are respectively pumped into the impinging flow reactor, and are rapidly mixed with the circulating material in the impinging flow reactor for complexation In the reactive extraction process, the circulating material rate is 200% of the feed amount. The operating temperature was controlled at 3 °C, the residence time was 10 min, and the reaction pressure was 1.5 MPa.
[0044] The experimental results showed that the recovery rate of m-xylene was 88wt%, and the purity of m-xylene was 99.6 wt%.
Embodiment 2
[0046] According to the method of Example 1, the difference is that the operating temperature is changed to 10°C.
[0047] The experimental results showed that the recovery rate of m-xylene was 83 wt%, and the purity of m-xylene was 99.5 wt%.
Embodiment 3
[0049] According to the method of embodiment 1, difference is that residence time becomes 5min.
[0050] The experimental results showed that the recovery rate of m-xylene was 86 wt %, and the purity of m-xylene was 99.7 wt %.
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