Light pressure-resistant buoyancy material for deep submergence vehicle and preparation method of buoyancy material

A technology of buoyancy materials and submersibles, which is applied in the field of marine engineering materials, can solve problems such as excessive buoyancy structure size, insufficient net buoyancy, and obstacles to submersible exploration, and achieve solidification at medium temperature, increase stirring efficiency, and excellent miscibility Effect

Inactive Publication Date: 2017-12-29
HARBIN ENG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the performance of domestic deep-water buoyancy materials is still in the development stage compared with foreign countries. Compared with foreign products of the same grade, there are still problems such as high density, low strength, high water absorption and low production efficiency, resulting in the producti

Method used

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  • Light pressure-resistant buoyancy material for deep submergence vehicle and preparation method of buoyancy material
  • Light pressure-resistant buoyancy material for deep submergence vehicle and preparation method of buoyancy material
  • Light pressure-resistant buoyancy material for deep submergence vehicle and preparation method of buoyancy material

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0025] Example 1:

[0026] Prepare light-weight pressure-resistant buoyancy materials for deep-sea submersibles according to the proportions in Table 1. The specific preparation methods are as follows:

[0027] (1) Measured in parts by mass, take 56 parts of bisphenol A epoxy resin, 14 parts of low viscosity modifier, 30 parts of reinforcing modifier, 50 parts of liquid organic acid anhydride curing agent and 4 parts of liquid imidazole The curing agent is added to the mixing container with stirring and turning, and stirred evenly to obtain a resin glue with low viscosity characteristics;

[0028] (2) Measured in parts by mass, take 32 parts of the dried hollow glass beads and add them to the mixer, and then add the resin glue obtained above into the mixer and stir in vacuum;

[0029] (3) The stirring process temperature is room temperature 25℃~30℃, the stirring speed is slowly increased from 0r / min to 30r / min, and the rising speed is controlled to increase by 1r / min every 2 seconds. ...

Example Embodiment

[0039] Example 2:

[0040] Prepare light-weight pressure-resistant buoyancy materials for deep-sea submersibles according to the proportions in Table 3. The specific preparation methods are:

[0041] (1) Measured in parts by mass, take 60 parts of bisphenol A epoxy resin, 20 parts of low viscosity modifier, 20 parts of reinforcing modifier, 45 parts of liquid organic anhydride curing agent and 6 parts of liquid imidazole The curing agent is added to the mixing container with stirring and turning, and evenly stirred to obtain a resin glue with low viscosity characteristics;

[0042] (2) Measured in parts by mass, take 33 parts of the dried hollow glass beads and add them to the mixer, and then add the resin glue obtained above into the mixer, and stir in vacuum;

[0043] (3) The stirring process temperature is room temperature 25℃~30℃, the stirring speed is slowly increased from 0r / min to 30r / min, and the rising speed is controlled to increase by 1r / min every 2 seconds. Start timing w...

Example Embodiment

[0053] Example 3:

[0054] Prepare light-weight pressure-resistant buoyancy materials for deep-sea submersibles according to the proportions in Table 5. The specific preparation methods are as follows:

[0055] (1) Measured in parts by mass, take 52 parts of bisphenol A epoxy resin, 10 parts of low viscosity modifier, 38 parts of reinforcing modifier, 55 parts of liquid organic acid anhydride curing agent and 3 parts of liquid imidazole The curing agent is added to the mixing container with stirring and turning, and stirred evenly to obtain a resin glue with low viscosity characteristics;

[0056] (2) Measured in parts by mass, take 32 parts of the dried hollow glass microbeads and add them to the mixer, and then add the resin glue obtained above into the mixer and stir in vacuum;

[0057] (3) The stirring process temperature is room temperature 25℃~30℃, the stirring speed is slowly increased from 0r / min to 30r / min, and the rising speed is controlled to increase by 1r / min every 2 seco...

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Abstract

The invention provides a light pressure-resistant buoyancy material for a deep submergence vehicle and a preparation method of the buoyancy material. The buoyancy material is prepared from, in parts by mass, 50-60 parts of bisphenol-A epoxy resin, 20-40 parts of a reinforced modifier, 10-20 parts of a low-viscosity modifier, 40-60 parts of a first curing agent, 2-8 parts of a second curing agent and 30-40 parts of hollow glass beads, wherein the reinforced modifier is hexahydrophthalic diglycidyl ester, the low-viscosity modifier is neopentyl glycol diglycidyl ether, the first curing agent is a liquid-state organic acid anhydride curing agent, and the second curing agent is a liquid-state imidazole curing agent. The prepared light pressure-resistant buoyancy material for the deep submergence vehicle has the density of 0.50-0.57 g/cm<3>, the compression strength reaching 40-60 MPa and the isostatic hydrostatic pressure water absorption rate smaller than 1% and can meet requirements of the deep sea submergence vehicle at 3,000-5,000 m underwater.

Description

technical field [0001] The invention relates to a marine engineering material, and also relates to a preparation method of the marine engineering material. Specifically, it is a light-weight pressure-resistant buoyancy material for deep-sea submersibles and a preparation method thereof. Background technique [0002] With the advancement of science and technology and the development of marine engineering, people have increased the depth of deep-sea exploration and oil drilling year by year, and at the same time put forward higher requirements for deep-water buoyancy materials for deep-sea submersibles. At present, deep sea exploration and development are mainly based on deep diving technology, using submersibles, underwater robots, etc. to conduct observation, sampling and underwater operations in the deep sea, and to maintain and install marine engineering instruments and facilities. High-strength light-weight pressure-resistant buoyancy materials are one of the important c...

Claims

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Application Information

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IPC IPC(8): C08L63/00C08K7/28C08K5/1515C08K5/1539
CPCC08K7/28C08K5/1515C08K5/1539C08K2201/003C08L63/00
Inventor 乔英杰邢志鹏张晓红王晓东
Owner HARBIN ENG UNIV
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