Method for producing asphalt warm mix wax
A warm mixing and asphalt technology, which is used in petroleum wax recovery, petroleum wax refining, climate change adaptation, etc., can solve the problems of reducing the mixing temperature of asphalt mixture, being difficult to separate, and reducing the viscosity of asphalt at 60°C.
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Embodiment 1
[0059] This embodiment includes: (A) emulsification and (B) sweating.
[0060] (A) Emulsification: Including (A1) oil phase material preparation, (A2) water phase material preparation, (A3) emulsion preparation three steps.
[0061] (A1) Oil phase material preparation:
[0062] Take polyethylene wax as a by-product of the polyethylene plant (China Petroleum Liaoyang Petrochemical Ethylene Plant, drop melting point 85.8°C; penetration (25°C) 52 (10 -1 mm); Penetration (55°C) > 200 (10 -1 mm). From the penetration at 25°C and 55°C, it can be seen that the raw material contains a large amount of low-melting point substances) 70.0Kg, after heating to 93°C and melting, add 2.1Kg diethylene glycol fatty acid ester, 1.0Kg sorbitan monopalm Ester and 0.5Kg lauryl betaine, be divided into two parts evenly after stirring.
[0063] (A2) Preparation of aqueous phase materials
[0064] Component (I) Preparation of water phase material: prepare HCl solution with a concentration of 3.3%...
Embodiment 2
[0084] This embodiment includes: (A) emulsification and (B) sweating.
[0085] (A) Emulsification: Including (A1) oil phase material preparation, (A2) water phase material preparation, (A3) emulsion preparation three steps.
[0086] (A1) Oil phase material preparation:
[0087] Take 73.0Kg of polyethylene wax (same as Example 1) produced by the polyethylene plant, heat to 89°C and melt, add 1.9Kg sorbitan monostearate, 0.7Kg diethylene glycol monolaurate and 0.4 Kg triacetamide oleate is divided into two parts evenly after stirring.
[0088] (A2) Preparation of aqueous phase materials
[0089] Preparation of component (I) water phase material: prepare H2 with a concentration of 2.0% 2 SO 4 Solution, take 12.0Kg and heat to 93°C;
[0090] Preparation of component (II) water phase material: prepare Na with a concentration of 2.2% 2 CO 3 Solution, take 12.0Kg and heat to 93°C.
[0091] (A3) Emulsion preparation
[0092] Preparation of component (I) emulsion: Stir one par...
Embodiment 3
[0098] This embodiment includes: (A) emulsification and (B) sweating.
[0099] (A) Emulsification: Including (A1) oil phase material preparation, (A2) water phase material preparation, (A3) emulsion preparation three steps.
[0100] (A1) Oil phase material preparation:
[0101] Take 78.0Kg of polyethylene wax (same as Example 1) produced by the polyethylene plant, heat to 91°C and melt, add 1.6Kg sorbitan monostearate, 0.5Kg diethylene glycol monolaurate and 0.3 Kg sodium maleic acid monoester sulfonate, stir evenly and divide into two parts on average.
[0102] (A2) Preparation of aqueous phase materials
[0103] Preparation of component (I) water phase material: prepare H2 with a concentration of 2.6% 2 SO 4 Solution, take 9.8Kg and heat to 93°C;
[0104] Preparation of component (II) water phase material: prepare K with a concentration of 3.2% 2 CO 3 Solution, take 9.8Kg and heat to 93°C.
[0105] (A3) Emulsion preparation
[0106] Preparation of component (I) emul...
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