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Etching method for silver-copper solder

An etching and soldering technology, applied in the field of surface treatment, can solve the problems of removal, silver migration, and increase of impurities, and achieve the effect of improving the working environment, reducing environmental pollution, and increasing the range

Active Publication Date: 2018-01-23
NO 55 INST CHINA ELECTRONIC SCI & TECHNOLOGYGROUP CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] 1) The brazing appearance of the shell does not meet the requirements, and the size is poor;
[0004] 2) The number of holes in the solder layer and the inclusion of impurities increase, and these impurities cannot be cleaned up during subsequent plating, resulting in an increase in the proportion of peeling and blistering after plating;
[0005] 3) The coating cannot fully wrap the solder well, resulting in the problem of silver migration;
[0006] 4) It may have a certain impact on other reliability of the device
However, there is currently no good way to etch the silver-copper solder specifically or preferentially so that the solder is removed from all parts of the product

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] A method for etching silver-copper solder, comprising the following steps:

[0039] ①Alkaline degreasing

[0040] Alkaline degreasing is an aqueous solution, which contains 40 g / L chemical degreasing powder, and the brazed semi-finished shell is placed in an alkaline degreasing solution at 60°C for 5 minutes;

[0041] ②Washing

[0042] Rinse the shell after alkaline degreasing with tap water for 3 minutes, and then wash it with deionized water for 3 minutes;

[0043] ③Pickling

[0044] The pickling solution is an aqueous solution, which contains: 5mL / L of OP emulsifier, 75g / L of thiourea, and 100mL / L of sulfuric acid. Put the washed shell into the pickling solution at 60°C for 5 minutes;

[0045] ④washing

[0046] Rinse the shell after alkaline degreasing with tap water for 3 minutes, and then wash it with deionized water for 3 minutes;

[0047] ⑤ drying

[0048] Use a 100°C high-temperature blast drying oven to dry the washed shell at high temperature;

[0049] ...

Embodiment 2

[0052] A method for etching silver-copper solder, comprising the following steps:

[0053] ①Alkaline degreasing

[0054] Alkaline degreasing is an aqueous solution, which contains 60 g / L chemical degreasing powder, and the brazed semi-finished shell is placed in an alkaline degreasing solution at 80°C for 15 minutes;

[0055] ②Washing

[0056] Rinse the shell after alkaline degreasing with tap water for 5 minutes, and then wash it with deionized water for 5 minutes;

[0057] ③Pickling

[0058] The pickling solution is an aqueous solution, which contains: 10mL / L of OP emulsifier, 150g / L of thiourea, and 200mL / L of sulfuric acid. Put the washed shell into the pickling solution at 80°C for 15 minutes;

[0059] ④washing

[0060] Rinse the shell after alkaline degreasing with tap water for 5 minutes, and then wash it with deionized water for 5 minutes;

[0061] ⑤ drying

[0062] Use a high-temperature blast drying oven at 120°C to dry the shell after washing at high temperatu...

Embodiment 3

[0066] A method for etching silver-copper solder, comprising the following steps:

[0067] ①Alkaline degreasing

[0068] Alkaline degreasing is an aqueous solution, which contains 50 g / L chemical degreasing powder, and the brazed semi-finished shell is placed in an alkaline degreasing solution at 70°C for 10 minutes;

[0069] ②Washing

[0070] Rinse the shell after alkaline degreasing with tap water for 4 minutes, and then wash it with deionized water for 4 minutes;

[0071] ③Pickling

[0072] The pickling solution is an aqueous solution, which contains: 7mL / L OP emulsifier, 115g / L thiourea, and 150mL / L sulfuric acid. Put the washed shell into the pickling solution at 70°C for 10 minutes;

[0073] ④washing

[0074] Rinse the shell after alkaline degreasing with tap water for 4 minutes, and then wash it with deionized water for 4 minutes;

[0075] ⑤ drying

[0076] Use a high-temperature blast drying oven at 110°C to dry the shell after washing at high temperature;

[00...

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Abstract

The invention relates to an etching method for silver-copper solder. The etching method comprises the following steps of (1) alkaline oil removal, specifically, a brazed semi-finished product outer shell is put into an alkaline oil removal solution to be cleaned up; (2) water washing, specifically, the brazed semi-finished product outer shell is washed by tap water firstly and then washed by usingdeionized water; (3) pickling, specifically, the water-washed outer shell is put into a pickling liquid to be washed; (4) drying, specifically, a high-temperature blast drying box is used for high-temperature drying the water-washed outer shell; (5) etching, specifically, the outer shell is placed in an etching solution; and (6) final processing, specifically, the outer shell is taken out after etching is finished, the step (2) water washing and the step (4) drying are repeated. The etching method has the advantages that (1) the silver-copper solder is etched without any corrosion damage, thecoverage of outer shell brazing appearance, size, solder and subsequent plating reliability are high; (2) the etching process is slowed down, and the etching time range is increased; (3) environmental pollution is relieved; (4) the etching method is low in cost, simple and easy to operate; and (5) the problem of silver displacement of radio frequency power device outer shells is solved, and the effect is remarkable.

Description

technical field [0001] The invention relates to an etching method of silver-copper solder, which belongs to the technical field of surface treatment. Through the method, the silver-copper solder can be selectively removed from all positions of the whole. This method is especially useful for obtaining the desired shell brazing shape, size, solder coverage and subsequent plating reliability. In addition, this method is especially critical as a pre-treatment for products with "silver migration" requirements . Background technique [0002] Silver-based solder is the longest and most widely used type of solder in solder. Especially the Ag-Cu eutectic (Ag72-Cu28) solder is currently the most widely used solder in the soldering process of electronic packaging devices. It has a low melting point, no crystallization interval, good fluidity, and the thermal conductivity and electrical conductivity of the formed weld Good performance, so in the manufacture of electronic packaging com...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23F1/44
Inventor 解瑞程凯谢新根杨建陈宇宁
Owner NO 55 INST CHINA ELECTRONIC SCI & TECHNOLOGYGROUP CO LTD
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