Composite lithium ion battery negative material Li3VO4/Ag and preparation method thereof
A lithium-ion battery and negative electrode material technology, applied in the field of electrochemical power supply, can solve the problems of poor conductivity, unsatisfactory electrochemical performance, and low Coulombic efficiency, and achieve the effects of easy operation, good cycle performance, and good repeatability
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Embodiment 1
[0018] The material synthesis steps are as follows:
[0019] 1) Weigh 1 mmol and 3 mmol of lithium carbonate and vanadium pentoxide according to the molar ratio of 1:3, respectively, and dissolve them in beakers A and B filled with 10 ml of deionized water, and stir on a magnetic stirrer for 20 minutes to fully dissolve;
[0020] 2) Weigh 5mmol hexamethylenetetramine and dissolve it in beaker C filled with 10ml deionized water, transfer the solutions in beakers B and C in step 1) to beaker A, stir on a magnetic stirrer for 40min to obtain the color homogeneous solution;
[0021] 3) Transfer the uniformly colored solution obtained in step 2) to the lining of a 50ml hydrothermal kettle and add deionized water to 80% of its volume, react in a blast oven at 120°C for 24h, and cool naturally to room temperature;
[0022] 4) Slowly add a theoretical silver content of Li to the product obtained in step 3) 3 VO 4 Quality 5% silver nitrate solution;
[0023] 5) Put the intermediate...
Embodiment 2
[0026] The material synthesis steps are as follows:
[0027] 1) Weigh 1 mmol and 3 mmol of lithium carbonate and vanadium pentoxide according to the molar ratio of 1:3, respectively, and dissolve them in beakers A and B filled with 10 ml of deionized water, and stir on a magnetic stirrer for 20 minutes to fully dissolve;
[0028] 2) Weigh 5mmol hexamethylenetetramine and dissolve it in beaker C filled with 10ml deionized water, transfer the solutions in beakers B and C in step 1) to beaker A, stir on a magnetic stirrer for 40min to obtain the color homogeneous solution;
[0029] 3) Transfer the uniformly colored solution obtained in step 2) to the lining of a 50ml hydrothermal kettle and add deionized water to 80% of its volume, react in a blast oven at 120°C for 24h, and cool naturally to room temperature;
[0030] 4) Slowly add a theoretical silver content of Li to the product obtained in step 3) 3 VO 4 Quality 5% silver nitrate solution;
[0031]5) Put the intermediate ...
Embodiment 3
[0034] The material synthesis steps are as follows:
[0035] 1) Weigh 1 mmol and 3 mmol of lithium carbonate and vanadium pentoxide according to the molar ratio of 1:3, respectively, and dissolve them in beakers A and B filled with 10 ml of distilled water, and stir on a magnetic stirrer for 20 minutes to fully dissolve;
[0036] 2) Weigh 5mmol of hexamethylenetetramine and dissolve it in beaker C containing 10ml of distilled water, transfer the solutions in beakers B and C in step 1) to beaker A, stir on a magnetic stirrer for 40min to obtain a uniform color solution;
[0037] 3) Transfer the homogeneously colored solution obtained in step 2) to the lining of a 50ml hydrothermal kettle to 80% volume, react in a blast oven at 120°C for 24 hours, and cool naturally to room temperature;
[0038] 4) in the product that obtains in step 3), add the silver nitrate that theoretical silver content is 5%;
[0039] 5) Put the intermediate product obtained in step 4) in an oil bath at ...
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