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High-temperature-resistant, high-toughness and sulfuration-resistant AMOLED packaging silica gel

A high-toughness, vulcanization-resistant technology, applied in adhesives, modified epoxy resin adhesives, electrical components, etc., can solve the problems of easy cracking of packaging materials, impact dead lights, and reduced toughness of materials, so as to achieve easy operation and durability Good high temperature performance and good weather resistance

Inactive Publication Date: 2018-02-09
HEFEI HUIKE JINYANG TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, in the formula design, methods such as increasing the content of phenyl silicone resin and increasing the crosslinking density are used to improve the vulcanization resistance. Although such a design improves the vulcanization resistance, the internal stress of the packaging material is too high, which will lead to a decrease in the toughness of the material. The reaction is in After encapsulation, high and low temperature cold and heat impact dead lights, and the encapsulation material is easy to crack after high and low temperature.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] Example 1 A vulcanization resistant AMOLED encapsulating silica gel with high temperature resistance and high toughness, which is composed of the following parts by weight of raw materials: 35 parts of hydrogen-terminated silicone resin, 26 parts of vinyl resin, and 15 parts of methylphenylsiloxane Parts, 7 parts of dimethylpolysiloxane monomer, 7 parts of divinyltetramethyldisiloxane, 6 parts of tetrabutylammonium hydroxide, 3 parts of catalyst, 4 parts of adhesive, 3 parts of crosslinking agent, 2 parts of inhibitor, 2 parts of curing accelerator and 3 parts of curing inhibitor.

[0020] A high-temperature and high-toughness vulcanization-resistant AMOLED encapsulating silica gel, and its preparation method includes the following steps:

[0021] (1) Mix hydrogen-terminated silicone resin, vinyl resin, methyl phenyl siloxane, dimethyl polysiloxane monomer, divinyl tetramethyl disiloxane, and tetrabutyl ammonium hydroxide. , Heat the mixture to 45°C for dispersion treatment...

Embodiment 2

[0030] Example 2 A high-temperature and high-toughness vulcanization-resistant AMOLED encapsulating silica gel, which is composed of the following parts by weight of raw materials: 44 parts by weight of hydrogen-terminated silicone resin, 32 parts of vinyl resin, and 26 parts of methylphenylsiloxane Parts, 11 parts of dimethyl polysiloxane monomer, 14 parts of divinyl tetramethyl disiloxane, 12 parts of tetrabutyl ammonium hydroxide, 6 parts of catalyst, 7 parts of adhesive, 5 parts of crosslinking agent, 4 parts of inhibitor, 3 parts of curing accelerator and 5 parts of curing inhibitor.

[0031] A high-temperature and high-toughness vulcanization-resistant AMOLED encapsulating silica gel, and its preparation method includes the following steps:

[0032] (1) Mix hydrogen-terminated silicone resin, vinyl resin, methyl phenyl siloxane, dimethyl polysiloxane monomer, divinyl tetramethyl disiloxane, and tetrabutyl ammonium hydroxide. , Heat the mixture to 45°C for dispersion treatmen...

Embodiment 3

[0041] Example 3 A high-temperature and high-toughness vulcanization-resistant AMOLED encapsulating silica gel, which is composed of the following parts by weight of raw materials: 38 parts by weight of hydrogen-terminated silicone resin, 31 parts of vinyl resin, and 22 parts of methylphenylsiloxane Parts, 9 parts of dimethylpolysiloxane monomer, 12 parts of divinyltetramethyldisiloxane, 9 parts of tetrabutylammonium hydroxide, 4 parts of catalyst, 6 parts of adhesive, 4 parts of crosslinking agent, 3 parts of inhibitor, 3 parts of curing accelerator and 4 parts of curing inhibitor.

[0042] A high-temperature and high-toughness vulcanization-resistant AMOLED encapsulating silica gel, and its preparation method includes the following steps:

[0043] (1) Mix hydrogen-terminated silicone resin, vinyl resin, methyl phenyl siloxane, dimethyl polysiloxane monomer, divinyl tetramethyl disiloxane, and tetrabutyl ammonium hydroxide. , Heat the mixture to 45°C for dispersion treatment for ...

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PUM

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Abstract

The invention discloses a high-temperature-resistant, high-toughness and sulfuration-resistant AMOLED packaging silica gel prepared from the following raw materials in parts by weight: 35-44 parts ofhydrogen-terminated silicone resin, 26-32 parts of vinyl resin, 15-26 parts of polymethylphenylsiloxane, 7-11 parts of dimethyl polysiloxane monomers, 7-14 parts of divinyltetramethyldisiloxane, 6-12parts of tetrabutyl ammonium hydroxide, 3-6 parts of catalyst, 4-7 parts of binder, 3-5 parts of crosslinking agent, 2-4 parts of inhibitor, 2-3 parts of curing accelerator and 3-5 parts of curing inhibitor. Compared with the prior art, the high-temperature-resistant, high-toughness and sulfuration-resistant AMOLED packaging silica gel has the beneficial effects that the AMOLED packaging silica gel is strong in sulfuration resistance, good in sealing performance and high temperature resistance, good in weather resistance, yellowing-resistant and easy to defoam and further has the advantages such as high toughness and convenience in operation in addition to excellent optical structure and high refractive index.

Description

Technical field [0001] The invention relates to the technical field of encapsulating silica gel, in particular to a vulcanization resistant AMOLED encapsulating silica gel with high temperature resistance and high toughness. Background technique [0002] The rise of the LED industry has brought new hopes for energy conservation, emission reduction, and environmental protection, and has demonstrated extremely broad application prospects. With the rapid development of the LED industry, especially the lighting industry, LEDs are gradually developing in the direction of high power, so more and more comprehensive requirements are put forward for packaging materials. High refractive index LED packaging silica gel has become an important packaging material because of its low internal stress, good aging resistance, high and low temperature resistance, and high luminous flux, and is widely used in the field of LED packaging. [0003] With the development of industry, the sulfur content in ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09J183/05C09J163/10C09J183/06C09J183/07H01L33/56
CPCC08K2201/014C08L2201/08C08L2203/206C08L2205/02C08L2205/025C08L2205/035C09J183/04H01L33/56C08L63/10C08L83/04C08L83/06
Inventor 白航空
Owner HEFEI HUIKE JINYANG TECH
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