A kind of lithium battery and preparation method thereof
A lithium battery and electrolyte technology, applied in the field of lithium battery and its preparation, can solve the problems of insufficient performance such as low conductivity theoretical specific capacity, energy efficiency ratio, energy density, etc., to improve energy efficiency ratio, improve charge-discharge efficiency and cycle performance, the effect of avoiding oxidation
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[0045] The present invention also provides a preparation method of a lithium battery, comprising the following steps:
[0046] (1) Preparation of positive electrode;
[0047] (2) preparation of negative electrode;
[0048] (3) After winding the positive electrode, negative electrode and separator, inject the electrolyte, then fill the lithium battery with an inert gas until the pressure is 0.3-3MPa, then stand the lithium battery at 20-35°C for 6-24h, and then Stand upright at 40-55°C for 6-24h, then vacuumize to a pressure of -0.08-0.05MPa and seal to obtain a lithium battery.
[0049] According to the present invention, in the preparation of the battery, during the infiltration process of the electrolyte, the pressure inside the battery is increased by injecting an inert gas so that the electrode sheet can be completely infiltrated by the electrolyte, thereby increasing the ion and electron density in the later charging and discharging process. Transmission efficiency, imp...
Embodiment 1
[0069] (1) Positive electrode preparation
[0070] 1.6kg PVDF was dissolved in 21kg NMP to obtain a PVDF glue solution with a mass concentration of 7%; 96.8kg carbon-coated lithium iron phosphate (volume average particle size distribution D50 was 10 μm, tap density 1.2g / cm 3 , The specific surface area is 15m 2 / g), 1kg conductive graphite, 0.6kg graphene and the above-mentioned PVDF glue were stirred evenly under the condition of 40°C vacuum degree≤-0.08MPa to prepare positive electrode slurry;
[0071] Coat the positive electrode slurry on the front and back sides of a graphene-coated aluminum foil with a thickness of 20 μm (graphene layer is 2 μm + aluminum foil with a thickness of 16 μm), then dry at 120 ° C, roll under a pressure of 1.6 MPa and then cut Slitting on the machine to obtain a positive electrode with a size of 2350mm×180mm×20μm, and an area density of 161g / m 2 , the compacted density is 2.3g / cm 3 positive pole.
[0072] (2) Negative electrode preparation ...
Embodiment 2
[0078] (1) Positive electrode preparation
[0079] 1.5kg PVDF was dissolved in 28.5kgNMP to obtain a PVDF glue solution with a mass concentration of 5%; 96.5kg carbon-coated lithium iron phosphate (volume average particle size distribution D50 was 12 μm, tap density 1g / cm 3 , the specific surface area is 10m 2 / g), 1kg conductive graphite, 1kg graphene and the above-mentioned PVDF glue were stirred evenly under the condition of 40°C vacuum degree≤-0.08MPa to prepare positive electrode slurry;
[0080] Coat the positive electrode slurry on the front and back sides of a graphene-coated aluminum foil with a thickness of 18 μm (graphene layer is 2 μm + aluminum foil with a thickness of 14 μm), then dry at 120 ° C, roll under a pressure of 1.6 MPa and then cut Slitting on the machine to obtain a positive electrode with a size of 5300mm×74mm×20μm, and an area density of 155g / m 2 , the compacted density is 2.4g / cm 3 positive pole.
[0081] (2) Negative electrode preparation
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