Zinc oxide nanorod preparation method

A technology of zinc oxide nanorods and zinc acetate dihydrate is applied in the field of preparation of zinc oxide nanorods to achieve the effects of obvious semiconductor characteristics, good repeatability and excellent piezoelectric performance

Inactive Publication Date: 2018-03-13
SHAANXI ALLIANCE LOGISTICS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Piezoelectric power generation devices based on ZnO nanomaterials have been successfully developed and applied in micro-nano electromechanical systems, but there are few studies on the application of piezoelectricity based on ZnO to textiles.

Method used

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Embodiment Construction

[0012] The preparation method of the zinc oxide nanorods of the present invention comprises the following steps: (1) dripping ammonia water into the aqueous solution of zinc acetate dihydrate and hexamethylenetetramine to obtain the seed liquid of zinc oxide; (2) adding the seed liquid The crystal liquid was placed in a water bath at 35°C and kept warm for 5 minutes; (3) First, use tweezers to pick up the fabric substrate and place it vertically in the seed crystal liquid to stand still, then pull the substrate out of the liquid surface at a uniform speed, and finally Place the fabric substrate soaked with the seed liquid on the surface in an oven, and anneal for 30 minutes to form a seed layer; (4) Turn on the constant temperature water bath, and when the temperature of the water bath reaches the temperature, put the fabric with the seed layer into the reaction chamber vertically In the solution, ensure that the substrate is completely immersed in the solution, and finally sea...

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PUM

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Abstract

The invention discloses a zinc oxide nanorod preparation method and belongs to the field of piezoelectric power generation textiles. The zinc oxide nanorod preparation is characterized by comprising the following steps: dropwise adding ammonium hydroxide into a zinc acetate dihydrate and hexamethylene tetramine water solution to obtain zinc oxide seed crystal liquor; putting the seed crystal liquor into a water bath pot; clamping a textile lining by tweezers, perpendicularly putting into the seed crystal liquor, standing, then pulling the lining out of the liquid level from the solution at a constant speed and finally putting the textile lining with the surface soaked by the seed crystal liquor into an oven to form a seed crystal layer; opening a constant-temperature water bath pot, perpendicularly putting the textile on which the seed crystal layer grows into reaction fluid and wholly soaking a flask into the constant-temperature water bath pot; washing by deionized water after growthfinishes and drying to prepare the zinc oxide nanorods. The zinc oxide nanorods grow and are prepared on the silver-coated textile lining, the nanorods are perpendicularly and tightly arranged on thesurface of the textile, the zinc oxide nanorods have the advantages of obviously semiconductor characteristics and good repetition, and obvious current intensified signals appearing in a zinc oxide growth area shows that the zinc oxide nanorods have excellent piezoelectric property.

Description

technical field [0001] The invention belongs to the field of piezoelectric power generation textiles, and in particular relates to a preparation method of zinc oxide nanorods. Background technique [0002] As the world's energy consumption continues to increase and traditional energy sources continue to decrease, scientists are working hard to find new energy sources to supplement future energy sources. In people's daily life, mechanical energy exists everywhere, such as sound waves of speech, bending of fingers, stretching of muscles, movement of footsteps, and flow of air. If these naturally existing mechanical energy can be converted into electrical energy through some kind of device, the energy problem can be alleviated to a certain extent, which is of great research value. Based on this assumption, a new class of self-driven nanodevices that do not require an external power source has emerged. [0003] As early as the 1960s, some people began to study zinc oxide, and ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01G9/02B82Y40/00
CPCB82Y40/00C01G9/02C01P2004/16
Inventor 刘秋丽
Owner SHAANXI ALLIANCE LOGISTICS
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